Zhao Yuanyuan, Qiao Simo, Zhu Xiaohui, Guo Jinnan, Peng Guanqun, Zhu Xiaoxia, Gu Ruolan, Meng Zhiyun, Wu Zhuona, Gan Hui, Guifang Dou, Jin Yiguang, Liu Shuchen, Sun Yunbo
Anhui Medical University, Hefei, 230000, China.
Beijing Institute of Radiation Medicine, Beijing, 100850, China.
Heliyon. 2024 May 11;10(10):e31143. doi: 10.1016/j.heliyon.2024.e31143. eCollection 2024 May 30.
In order to investigate the effects of different drying methods on the properties of porous starch. The present study used four drying methods, namely hot air drying (HD), spray drying (SPD), vacuum freeze drying (FD) and supercritical carbon dioxide drying (SCD) to prepare maize and kudzu porous starch. Findings indicated that the physicochemical properties (e.g., morphology, crystallinity, enthalpy value, porosity, surface area and water absorption capacity as well as dye absorption capacity, particle size) of porous starch were significantly affected by the drying method. Compared with other samples, SCD-treated porous starch exhibited the highest surface areas of the starch (2.943 and 3.139 m/g corresponding to kudzu and maize, respectively), amylose content (22.02 % and 16.85 % corresponding to kudzu and maize, respectively), MB and NR absorption capacity (90.63 %, 100.26 % and 90.63 %, 100.26 %, corresponding to kudzu ad maize, respectively), and thermal stability, whereas HD-treated porous starch showed the highest water-absorption capacity (123.8 % and 131.31 % corresponding to kudzu and maize, respectively). The dye absorption of the maize and kudzu porous starch was positively correlated with surface area, according to Pearson's correlation analysis. Therefore, in this study, our aim was to explore the effects of different drying methods on the Structure and properties of porous starch, and provide reference for selecting the best drying method for its application in different fields.
为了研究不同干燥方法对多孔淀粉性质的影响。本研究采用四种干燥方法,即热风干燥(HD)、喷雾干燥(SPD)、真空冷冻干燥(FD)和超临界二氧化碳干燥(SCD)来制备玉米和葛根多孔淀粉。研究结果表明,干燥方法对多孔淀粉的物理化学性质(如形态、结晶度、焓值、孔隙率、表面积和吸水能力以及染料吸附能力、粒径)有显著影响。与其他样品相比,经SCD处理的多孔淀粉具有最高的淀粉表面积(葛根和玉米分别为2.943和3.139 m/g)、直链淀粉含量(葛根和玉米分别为22.02%和16.85%)、亚甲基蓝(MB)和中性红(NR)吸附能力(葛根和玉米分别为90.63%、100.26%和90.63%、100.26%)以及热稳定性,而经HD处理的多孔淀粉具有最高的吸水能力(葛根和玉米分别为123.8%和131.31%)。根据皮尔逊相关性分析,玉米和葛根多孔淀粉的染料吸附与表面积呈正相关。因此,在本研究中,我们的目的是探索不同干燥方法对多孔淀粉结构和性质的影响,并为其在不同领域的应用选择最佳干燥方法提供参考。