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钒酸银和石墨烯改性丙烯酸树脂的结构-性能相关性

Structure-properties correlation of acrylic resins modified with silver vanadate and graphene.

作者信息

Sahm Beatriz Danieletto, Ferreira Izabela, Carvalho-Silva João Marcos, Vilela Teixeira Ana Beatriz, Uchôa Teixeira Jean Valdir, Lisboa-Filho Paulo Noronha, Alves Oswaldo Luiz, Cândido Dos Reis Andréa

机构信息

Departament of Dental Materials and Prosthesis, Ribeirão Preto School of Dentistry, University of São Paulo (USP), Ribeirão Preto, SP, Brazil.

Paulista State University Júlio de Mesquita Filho (UNESP), Bauru, SP, Brazil.

出版信息

Heliyon. 2024 May 28;10(11):e32029. doi: 10.1016/j.heliyon.2024.e32029. eCollection 2024 Jun 15.

DOI:10.1016/j.heliyon.2024.e32029
PMID:38868038
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11168394/
Abstract

This study aimed to incorporate β-AgVO and rGO into self-curing (SC) and heat-curing (HC) acrylic resins and to evaluate their physicochemical, mechanical, and antimicrobial properties while correlating them with the characterized material structure. Acrylic resin samples were prepared at 0 % (control), 0.5 %, 1 %, and 3 % for both nanoparticles. The microstructural characterization was assessed by scanning electron microscopy (SEM) (n = 1) and energy dispersive X-ray spectroscopy (EDS) (n = 1). The physicochemical and mechanical tests included flexural strength (n = 10), Knoop hardness (n = 10), roughness (n = 10), wettability (n = 10), sorption (n = 10), solubility (n = 10), porosity (n = 10), and color evaluation (n = 10). The microbiological evaluation was performed by counting colony-forming units (CFU/mL) and cell viability (n = 8). The results showed that the β-AgVO samples showed lower counts of , , and due to their promising physicochemical properties. The mechanical properties were maintained with the addition of β-AgVO. The rGO samples showed higher counts of microorganisms due to the increase in physicochemical properties. It can be concluded that the incorporation of β-AgVO into acrylic resins could be an alternative to improve the antimicrobial efficacy and performance of the material.

摘要

本研究旨在将β - 钒酸银(β - AgVO)和还原氧化石墨烯(rGO)掺入自凝(SC)和热凝(HC)丙烯酸树脂中,并评估它们的物理化学、机械和抗菌性能,同时将这些性能与所表征的材料结构相关联。两种纳米颗粒均按0%(对照)、0.5%、1%和3%的比例制备丙烯酸树脂样品。通过扫描电子显微镜(SEM)(n = 1)和能量色散X射线光谱(EDS)(n = 1)对微观结构进行表征。物理化学和机械测试包括弯曲强度(n = 10)、努氏硬度(n = 10)、粗糙度(n = 10)、润湿性(n = 10)、吸附(n = 10)、溶解度(n = 10)、孔隙率(n = 10)和颜色评估(n = 10)。通过计数菌落形成单位(CFU/mL)和细胞活力(n = 8)进行微生物学评估。结果表明,β - AgVO样品因其良好的物理化学性质,显示出较低的[具体微生物名称1]、[具体微生物名称2]和[具体微生物名称3]数量。添加β - AgVO后机械性能得以保持。rGO样品由于物理化学性质的增加,显示出较高的微生物数量。可以得出结论,将β - AgVO掺入丙烯酸树脂中可能是提高材料抗菌功效和性能的一种替代方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/dbb4606e0283/gr11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/2848f9eb1d98/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/f44e3f2feab9/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/9528f7112c5b/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/e080456474ae/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/ec06f8a0e236/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/62b874a2834a/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/8e24455c0d47/gr7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/6206f8d31ea5/gr8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/a9cd7338aa7e/gr9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/76a64c2b8d6b/gr10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/dbb4606e0283/gr11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/2848f9eb1d98/gr1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/f44e3f2feab9/gr2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/9528f7112c5b/gr3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/e080456474ae/gr4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/ec06f8a0e236/gr5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/62b874a2834a/gr6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/8e24455c0d47/gr7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/6206f8d31ea5/gr8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/a9cd7338aa7e/gr9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/76a64c2b8d6b/gr10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/70fe/11168394/dbb4606e0283/gr11.jpg

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