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通过调控选择性激光熔化的体积能量密度在一种新型近β钛合金中实现等轴转变和优异力学性能

Achieving Equiaxed Transition and Excellent Mechanical Properties in a Novel Near-β Titanium Alloy by Regulating the Volume Energy Density of Selective Laser Melting.

作者信息

Li Xiaofei, Cheng Huanhuan, Shi Chengcheng, Liu Rui, Wang Ruyue, Yang Chuan

机构信息

School of Mechanical Engineering, Shandong University of Technology, Zibo 255000, China.

Luoyang Ship Material Research Institute, Luoyang 471023, China.

出版信息

Materials (Basel). 2024 May 29;17(11):2631. doi: 10.3390/ma17112631.

Abstract

This research investigated the relationship between volume energy density and the microstructure, density, and mechanical properties of the Ti-5Al-5Mo-3V-1Cr-1Fe alloy fabricated via the SLM process. The results indicate that an increase in volume energy density can promote a transition from a columnar to an equiaxed grain structure and suppress the anisotropy of mechanical properties. Specifically, at a volume energy density of 83.33 J/mm, the average aspect ratio of β grains reached 0.77, accompanied by the formation of numerous nano-precipitated phases. Furthermore, the relative density of the alloy initially increased and then decreased as the volume energy density increased. At a volume energy density of 83.33 J/mm, the relative density reached 99.6%. It is noteworthy that an increase in volume energy density increases the β grain size. Consequently, with a volume energy density of 83.33 J/mm, the alloy exhibited an average grain size of 63.92 μm, demonstrating optimal performance with a yield strength of 1003.06 MPa and an elongation of 18.16%. This is mainly attributable to the fact that an increase in volume energy density enhances thermal convection within the molten pool, leading to alterations in molten pool morphology and a reduction in temperature gradients within the alloy. The reduction in temperature gradients promotes equiaxed grain transformation and grain refinement by increasing constitutive supercooling at the leading edge of the solid-liquid interface. The evolution of molten pool morphology mainly inhibits columnar grain growth and refines grain by changing the grain growth direction. This study provided a straightforward method for inhibiting anisotropy and enhancing mechanical properties.

摘要

本研究调查了通过选择性激光熔化(SLM)工艺制备的Ti-5Al-5Mo-3V-1Cr-1Fe合金的体积能量密度与微观结构、密度及力学性能之间的关系。结果表明,体积能量密度的增加可促进柱状晶向等轴晶结构的转变,并抑制力学性能的各向异性。具体而言,在体积能量密度为83.33 J/mm时,β晶粒的平均长径比达到0.77,同时伴有大量纳米析出相的形成。此外,合金的相对密度随体积能量密度的增加先升高后降低。在体积能量密度为83.33 J/mm时,相对密度达到99.6%。值得注意的是,体积能量密度的增加会增大β晶粒尺寸。因此,在体积能量密度为83.33 J/mm时,该合金的平均晶粒尺寸为63.92 μm,屈服强度为1003.06 MPa,伸长率为18.16%,表现出最佳性能。这主要归因于体积能量密度的增加增强了熔池内的热对流,导致熔池形态发生变化,并降低了合金内部的温度梯度。温度梯度的降低通过增加固液界面前沿的本构过冷度促进了等轴晶转变和晶粒细化。熔池形态的演变主要通过改变晶粒生长方向抑制柱状晶生长并细化晶粒。本研究提供了一种抑制各向异性和提高力学性能的简便方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3606/11173926/eee7dda471f3/materials-17-02631-g001.jpg

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