Yang Ruirui, Chen Keyu, Wen Shifeng, Zhu Shijie, Qin Haotian, Wu Xiaochao, Zhou Yan, Che Yusi, Shi Yusheng, He Jilin
Zhongyuan Critical Metals Laboratory, Zhengzhou 450001, China.
School of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, China.
Materials (Basel). 2022 Aug 25;15(17):5863. doi: 10.3390/ma15175863.
AS41 magnesium alloy possesses outstanding performance features such as light weight, high strength to toughness ratio and excellent heat resistance due to the addition of Si element, while traditional casting methods are prone to inducing large grain size and coarse MgSi phase. In this study, we first reported utilizing the selective laser melting (SLM) technique, fabricating AS41 samples and exploring the effect of laser energy densities on the metallurgical quality by characterizing and investigating the microstructure and mechanical properties. Results showed that the optimal laser energy density range was 60 to 100 J/mm. Average grain size of only 2.9 μm was obtained with weak texture strength of 1.65 in {0001} orientation. Meanwhile, many dispersed secondary β-MgAl and MgSi phases were distributed inside the α-Mg matrix. It was confirmed that the SLM process introduced more grain recrystallization, inducing giant high-angle grain boundaries (HAGBs) and hindering the movement of dislocations, therefore forming dislocation strengthening while achieving grain refinement strengthening. Finally, three times the ultimate tensile strength of 313.7 MPa and higher microhardness of 96.4 HV than those of the as-cast state were obtained, verifying that the combined effect of grain refinement, solid solution strengthening and precipitation strengthening was responsible for the increased strength. This work provides new insight and a new approach to preparing AS41 magnesium alloy.
AS41镁合金由于添加了硅元素而具有诸如重量轻、强度韧性比高和耐热性优异等突出性能特点,而传统铸造方法容易导致晶粒尺寸大且MgSi相粗大。在本研究中,我们首次报道了利用选择性激光熔化(SLM)技术制备AS41样品,并通过表征和研究微观结构及力学性能来探索激光能量密度对冶金质量的影响。结果表明,最佳激光能量密度范围为60至100 J/mm。获得了平均晶粒尺寸仅为2.9μm且{0001}取向织构强度为1.65的弱织构。同时,许多弥散分布的次生β-MgAl和MgSi相分布在α-Mg基体内部。证实了SLM工艺引入了更多的晶粒再结晶,产生了巨大的大角度晶界(HAGBs)并阻碍了位错的运动,从而在实现晶粒细化强化的同时形成了位错强化。最终,获得了比铸态下极限抗拉强度高两倍且显微硬度高96.4 HV的性能,验证了晶粒细化、固溶强化和析出强化的综合作用导致了强度的提高。这项工作为制备AS41镁合金提供了新的见解和新方法。