Qu Zhiwei, Lei Min, Chen Guohua, Huang Chaowen, Liu Dan, Luo Ai
College of Materials and Metallurgy, Guizhou University, Guiyang 550025, China.
Key Laboratory for Materials Structure and Strength of Guizhou Province, Guiyang 550025, China.
Materials (Basel). 2024 Jun 2;17(11):2690. doi: 10.3390/ma17112690.
In this study, the decomposition of a martensite/austenite (M/A) microconstituent in bainitic steels was analyzed using differential scanning calorimetry (DSC) data in conjunction with Kissinger's and Johnson-Mehl-Avrami-Kolmogorov (JMAK)'s formulas. In bainitic steel subjected to austempering heat treatment, the presence of an M/A microstructure adversely affects the mechanical properties. According to the kinetic equations derived, it is observed that after tempering the sample at 600 °C for 4000 s, the generation of each phase reaches its maximum. The SEM images taken before and after tempering reveal extensive decomposition of the M/A constituent in the microstructure. The proportion of the M/A microstructure decreased significantly from about 10% before tempering to less than 1% after. Additionally, the content of residual austenite also reduced nearly to zero. These observations are consistent with the predictions of the kinetic equations.
在本研究中,结合基辛格公式和约翰逊-梅hl-阿夫拉米-科尔莫戈罗夫(JMAK)公式,利用差示扫描量热法(DSC)数据对贝氏体钢中马氏体/奥氏体(M/A)微结构的分解进行了分析。在进行等温淬火热处理的贝氏体钢中,M/A微结构的存在会对力学性能产生不利影响。根据推导的动力学方程,观察到在600℃下对样品回火4000 s后,各相的生成达到最大值。回火前后拍摄的扫描电子显微镜(SEM)图像显示,微结构中的M/A组分发生了广泛分解。M/A微结构的比例从回火前的约10%显著降低至回火后的不到1%。此外,残余奥氏体的含量也几乎降至零。这些观察结果与动力学方程的预测一致。