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热处理对选择性激光熔化制备的CX不锈钢微观结构和力学性能的影响

Effect of heat treatment on the microstructure and mechanical properties of CX stainless steel fabricated by selective laser melting.

作者信息

Wu Shaoqian, Wang Tianshu, Wu Shuo, Xing Shilong, Hou Jiabin, Zhao Yuantao, Li Zongan, Liu Yanbo

机构信息

School of Navigation and Shipping, Shandong Jiaotong University, Weihai, 264209, People's Republic of China.

School of Construction Machinery, Shandong Jiaotong University, Jinan, 250357, People's Republic of China.

出版信息

Sci Rep. 2025 Sep 1;15(1):32257. doi: 10.1038/s41598-025-17582-1.

DOI:10.1038/s41598-025-17582-1
PMID:40890325
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12402176/
Abstract

A novel Corrax (CX) stainless steel was fabricated using the Selective Laser Melting (SLM) process. This study examined the influence of heat treatment processes on the microstructure and mechanical properties of CX stainless steel. Results indicate that SLM-fabricated CX samples mainly consist of martensite and residual austenite, with tensile strength and hardness of 1124 MPa and 337.4 HV, respectively. After solution treatment at 850 °C for 0.5 h (ST), the sample exhibited the highest martensite content, with nearly all residual austenite eliminated. Nickel and aluminum are fully dissolved within the matrix, leading to a supersaturated solid solution. This martensitic structure with a high dislocation density lays an important foundation for the subsequent aging treatment. Subsequent aging treatments at various temperatures demonstrate that when CX samples are subjected to solution aging at 850 °C for 0.5 h followed by aging at 525 °C for 4 h (ST + AT), all residual austenite is fully converted to martensite. The elements dissolved during the solution treatment precipitate, forming NiAl intermetallic compounds. This process leads to a substantial increase in tensile strength and surface hardness, achieving values of 1743 MPa and 526.8 HV, respectively. These results indicate that the solution and aging heat treatment significantly enhances the overall performance of CX samples.

摘要

采用选择性激光熔化(SLM)工艺制备了一种新型的科拉克斯(CX)不锈钢。本研究考察了热处理工艺对CX不锈钢微观结构和力学性能的影响。结果表明,经SLM制备的CX样品主要由马氏体和残余奥氏体组成,其抗拉强度和硬度分别为1124兆帕和337.4维氏硬度。在850℃下进行0.5小时的固溶处理(ST)后,样品的马氏体含量最高,几乎所有残余奥氏体都被消除。镍和铝完全溶解在基体中,形成过饱和固溶体。这种具有高位错密度的马氏体结构为后续的时效处理奠定了重要基础。在不同温度下进行的后续时效处理表明,当CX样品在850℃下进行0.5小时的固溶时效处理,然后在525℃下时效4小时(ST + AT)时,所有残余奥氏体都完全转变为马氏体。在固溶处理过程中溶解的元素析出,形成NiAl金属间化合物。这一过程导致抗拉强度和表面硬度大幅提高,分别达到1743兆帕和526.8维氏硬度。这些结果表明,固溶和时效热处理显著提高了CX样品的整体性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/6ab680fe1b13/41598_2025_17582_Fig13_HTML.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/3219e2c25711/41598_2025_17582_Fig9_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/c0547fdb112c/41598_2025_17582_Fig10_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/7c5b9b9dff57/41598_2025_17582_Fig11_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/9c5349e91342/41598_2025_17582_Fig12_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a9a4/12402176/6ab680fe1b13/41598_2025_17582_Fig13_HTML.jpg

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