da Silva Priscila Luciane, Bittencourt Hélio Radke, Burnett Luiz Henrique, Spohr Ana Maria
Department of Restorative Dentistry, Pontifical Catholic University of Rio Grande do Sul, School of Dentistry, Porto Alegre, Brazil.
Department of Statistics, Pontifical Catholic University of Rio Grande do Sul, Polytechnic School, Porto Alegre, Brazil.
J Esthet Restor Dent. 2024 Oct;36(10):1452-1458. doi: 10.1111/jerd.13283. Epub 2024 Jul 17.
To evaluate the in vitro influence of prior silane application on the microshear bond strength (μSBS) of Scotchbond Universal Plus to glass ceramic.
Thirty blocks of lithium disilicate ceramic were etched with hydrofluoric acid for 20 s and distributed into Group 1 (no silane and no adhesive), Group 2 (adhesive), Group 3 (silane + adhesive). Three cylinders of resin cement were made on each ceramic block. Five blocks (n = 15 cylinders) were subjected to the μSBS test after 24 h, and the other five blocks (n = 15 cylinders) were tested after 6 months of water storage.
According to two-way ANOVA, followed by Tukey's test, the means of μSBS (MPa), denoted by different letters, show significant differences (p < 0.05): after 24 h-Group 1 (31.7), Group 2 (43.3), and Group 3 (31.3); after 6 months-Group 1 (14.8), Group 2 (33.6), and Group 3 (30.3). After 6 months of storage, there was a significant decrease in μSBS for Groups 1 and 2, along with an increase in adhesive failures across all groups.
Prior application of silane did not increase the μSBS between Scotchbond Universal Plus and ceramic, and there was degradation at the bond interface over time.
Prior application of a silane agent is not necessary when using Scotchbond Universal Plus for bonding to glass ceramics. Regardless of the prior application of silane, there is degradation at the bond interface over time.
评估预先应用硅烷对Scotchbond Universal Plus与玻璃陶瓷之间微拉伸粘结强度(μSBS)的体外影响。
将30块二硅酸锂陶瓷用氢氟酸蚀刻20秒,分为第1组(无硅烷且无粘结剂)、第2组(粘结剂)、第3组(硅烷+粘结剂)。在每个陶瓷块上制作三个树脂水门汀圆柱体。五个块体(n = 15个圆柱体)在24小时后进行μSBS测试,另外五个块体(n = 15个圆柱体)在储存6个月后进行测试。
根据双向方差分析,随后进行Tukey检验,μSBS(MPa)的均值,用不同字母表示,显示出显著差异(p < 0.05):24小时后 - 第1组(31.7)、第2组(43.3)和第3组(31.3);6个月后 - 第1组(14.8)、第2组(33.6)和第3组(30.3)。储存6个月后,第1组和第2组的μSBS显著降低,所有组的粘结失败率增加。
预先应用硅烷并未增加Scotchbond Universal Plus与陶瓷之间的μSBS,且随着时间推移粘结界面会发生降解。
使用Scotchbond Universal Plus粘结玻璃陶瓷时,无需预先应用硅烷剂。无论是否预先应用硅烷,随着时间推移粘结界面都会发生降解。