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体外评价染色液对聚醚醚酮、整体氧化锆和树脂纳米陶瓷颜色和表面粗糙度的影响。

In Vitro Evaluation of Color and Surface Roughness Changes of Polyetheretherketone, Monolithic Zirconia, and Resin Nanoceramics Exposed to Staining Liquids.

机构信息

Balgat Oral and Dental Health Center, Ankara, Türkiye.

Private Practice, Çankaya, Ankara, Türkiye.

出版信息

Niger J Clin Pract. 2024 Jul 1;27(7):918-924. doi: 10.4103/njcp.njcp_259_24. Epub 2024 Jul 27.

Abstract

BACKGROUND

This study aims to investigate color stability and surface roughness of polyetheretherketone (PEEK), zirconia, and hybrid ceramics while stored in different liquids.

METHODS

A total of 240 specimens were prepared from monolithic zirconia, PEEK, and hybrid ceramics. All specimens were polished using rubber sets with different grain sizes. Color parameters (L*, a*, b*) were measured three times using a dental spectrophotometer in standard D65 lightning. Each group was divided into eight different groups to be kept in eight different solutions as distilled water, cola, red wine, tea, coffee, heptane, citric acid, and 50% ethanol. Specimens were held in solutions at 37°C for 12 days. Color measurements were repeated, and color change (ΔE) was calculated using the CIE Lab formula.

RESULTS

The color difference of PEEK specimens was found above the clinically acceptable limit; however, color differences for monolithic zirconia produced by coffee were found within the clinically acceptable limits. ZR and HC specimens' color change values were found between threshold values (1<ΔE < 3.3). The differences observed in surface roughness levels amongst the ZR specimens could be caused by the polishing instrument and procedure.

CONCLUSION

The color change of the materials was within acceptable limits, whereas the surface roughness increased more than 0.2 µm. Especially cola, heptane, and red wine significantly increased the mean surface roughness.

摘要

背景

本研究旨在研究聚醚醚酮(PEEK)、氧化锆和混合陶瓷在储存在不同液体中的颜色稳定性和表面粗糙度。

方法

从整体氧化锆、PEEK 和混合陶瓷中制备了 240 个样本。所有样本均使用不同粒度的橡胶套进行抛光。使用标准 D65 照明的口腔分光光度计三次测量颜色参数(L*、a*、b*)。将每组分为 8 个不同的组,分别保存在 8 种不同的溶液中,分别为蒸馏水、可乐、红酒、茶、咖啡、庚烷、柠檬酸和 50%乙醇。将样本在 37°C 的溶液中保存 12 天。重复颜色测量,并使用 CIE Lab 公式计算颜色变化(ΔE)。

结果

PEEK 样本的色差超过临床可接受范围;然而,咖啡产生的整体氧化锆样本的色差在临床可接受范围内。ZR 和 HC 样本的颜色变化值在阈值(1<ΔE < 3.3)之间。ZR 样本表面粗糙度水平的差异可能是由抛光仪器和程序引起的。

结论

材料的颜色变化在可接受范围内,而表面粗糙度增加超过 0.2 µm。特别是可乐、庚烷和红酒显著增加了平均表面粗糙度。

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