Zulfa Liyana Labiba, Rizaldi Wafiq Azhar, Azhar Jauhari, Safrida Ninik, Pratama Azzah Dyah, Wahyuono Ruri Agung, Fajarin Rindang, Hakim Arif Nur
Department of Materials and Metallurgical Engineering, Faculty of Industrial Technology and Systems Engineering, Institut Teknologi Sepuluh Nopember Jl. Arif Rahman Hakim, Kampus ITS Keputih-Sukolilo Surabaya 60111 Indonesia
Department of Chemistry, Faculty of Science and Data Analytics, Institut Teknologi Sepuluh Nopember Jl. Arif Rahman Hakim, Kampus ITS Keputih-Sukolilo Surabaya 60111 Indonesia.
RSC Adv. 2024 Aug 6;14(34):24687-24702. doi: 10.1039/d4ra03620d. eCollection 2024 Aug 5.
Thermal conductivity and adhesion strength effects were studied for thermal barrier coatings (TBCs) with different particle sizes, YSZ content, time, and temperature curing. The study involves three stages. The first step focuses on the characteristics of YSZ/polysilazane as the TBC, which is characterized using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR), X-Ray Diffraction (XRD), and Thermal Gravimetric Analysis (TGA). The second and third steps assess thermal conductivity and adhesion strength based on variables such as particle size, YSZ/polysilazane, time, and curing temperature. Results show that there was a synergistic effect between particle size-YSZ content and time-temperature curing to obtain specimens with good thermal properties. SB270/70 showed the lowest temperature compared to other specimens, up to 160 °C. Furthermore, YSZ/polysilazane thermal conductivity and adhesion properties could be enhanced by a prolonged curing time and higher temperature. This study emphasizes that the modification of particle size, YSZ content, time, and temperature curing is a promising strategy to improve the thermal properties of TBCs.
研究了不同粒径、YSZ含量、固化时间和温度的热障涂层(TBC)的热导率和粘附强度效应。该研究包括三个阶段。第一步聚焦于作为热障涂层的YSZ/聚硅氮烷的特性,采用扫描电子显微镜(SEM)、傅里叶变换红外光谱(FTIR)、X射线衍射(XRD)和热重分析(TGA)对其进行表征。第二步和第三步基于粒径、YSZ/聚硅氮烷、时间和固化温度等变量评估热导率和粘附强度。结果表明,粒径-YSZ含量与时间-温度固化之间存在协同效应,以获得具有良好热性能的试样。与其他试样相比,SB270/70显示出最低温度,高达160°C。此外,延长固化时间和提高温度可增强YSZ/聚硅氮烷的热导率和粘附性能。本研究强调,粒径、YSZ含量、时间和固化温度的改性是改善热障涂层热性能的一种有前景的策略。