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作为一种新型环保牙科修复材料的亲水性纤维与虾壳组合的力学性能及配方

Mechanical properties and formulation of hydrophilic fiber and shrimp shell combination as a novel eco-friendly dental restoration material.

作者信息

Fadhila Dewi Nur, Ridwan Alisha Zafirah, Amir Nur Aqilah, Abdillah Andi, Kartini N Ratih, H Hasanuddin, Djamaluddin Nursyamsi

机构信息

Dental Education Study Program, Faculty of Dentistry, Hasanuddin University, Indonesia.

Pharmacy Study Program, Faculty of Pharmacy, Hasanuddin University, Indonesia.

出版信息

Heliyon. 2024 Jul 5;10(14):e34180. doi: 10.1016/j.heliyon.2024.e34180. eCollection 2024 Jul 30.

Abstract

This study evaluates the mechanical properties and formulation of dental restoration material comprised of cellulose acetate (CA) from water hyacinth and chitosan (C) from white shrimp shells. The research phases included extraction, formulation, functional group testing, antibacterial, toxicity, water absorption and solubility, compressive, shear, tensile, hardness, microleakage, thermal expansion, and shrinkage. The experimental data were analyzed using probit regression, one-way ANOVA, and Kruskal-Wallis test. The data showed that CA and C had microxyl and amine groups, could inhibit , and were non-toxic. Composite resins were divided into nine formulations with different concentrations: F1 (1 % CA + 3 % C), F2 (1 % CA + 5 % C), F3 (1 % CA + 7 % C), F4 (3 % CA + 3 % C), F5 (3 % CA + 5 % C), F6 (3 % CA + 7 % C), F7 (5 % CA + 3 % C), F8 (5 % CA + 5 % C), and F9 (5 % CA + 7 % C). The F9 has mechanical strength close to the control group, with 113.33 μg/mm absorption, 80 μg/mm solubility, 32.67 Mpa compressive strength, 17.18 Mpa tensile strength, and no shrinkage. It shows that F9 has potential as an eco-friendly dental filling material. The present study completed the development of a formulation for a restoration material by combining water hyacinth fiber and shrimp skin chitosan. The outcomes of a comparative analysis of the mechanical properties of synthetic composite resins and water hyacinth fiber composites containing shrimp skin chitosan revealed that the F9 formulation (CA 5 % + C 7 %) exhibited the following fiber: absorption, compressive strength, tensile strength, hardness, and thermal expansion.

摘要

本研究评估了由水葫芦中的醋酸纤维素(CA)和白虾壳中的壳聚糖(C)组成的牙科修复材料的力学性能和配方。研究阶段包括提取、配方、官能团测试、抗菌、毒性、吸水性和溶解性、压缩、剪切、拉伸、硬度、微渗漏、热膨胀和收缩。使用概率回归、单因素方差分析和克鲁斯卡尔 - 沃利斯检验对实验数据进行分析。数据表明,CA和C具有微木糖基和胺基,能够抑制 ,且无毒。复合树脂分为九种不同浓度的配方:F1(1% CA + 3% C)、F2(1% CA + 5% C)、F3(1% CA + 7% C)、F4(3% CA + 3% C)、F5(3% CA + 5% C)、F6(3% CA + 7% C)、F7(5% CA + 3% C)、F8(5% CA + 5% C)和F9(5% CA + 7% C)。F9的机械强度接近对照组,吸水率为113.33μg/mm,溶解度为80μg/mm,抗压强度为32.67MPa,抗拉强度为17.18MPa,且无收缩。这表明F9有潜力作为一种环保型牙科填充材料。本研究通过将水葫芦纤维和虾皮壳聚糖结合,完成了一种修复材料配方的开发。对合成复合树脂和含虾皮壳聚糖的水葫芦纤维复合材料的力学性能进行比较分析的结果表明,F9配方(CA 5% + C 7%)在纤维方面表现出以下性能:吸水率、抗压强度、抗拉强度、硬度和热膨胀。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4b5b/11305253/6cd2ae9b9896/gr1.jpg

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