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沉淀剂对CeO纳米颗粒的促氧化和抗菌性能的影响——一项实验研究。

Effect of precipitant on pro-oxidative and antibacterial properties of CeO nanoparticles - an experimental study.

作者信息

Maddheshiya Shilpa, Rajwani Priyanka, Nara Seema

机构信息

Department of Biotechnology, Motilal Nehru National Institute of Technology Allahabad 211004 UP India

出版信息

Nanoscale Adv. 2024 Jul 29;6(19):4956-68. doi: 10.1039/d4na00234b.

Abstract

In this study, the synthesis of pro-oxidative cerium-oxide nanozymes (CeO NZs) is reliably performed the co-precipitation method using ceric ammonium nitrate as a precursor and ammonium carbonate as a precipitating agent. Different samples of CeO NZs were prepared by varying the amount of the precipitant. The synthesized NZs were characterized by ultraviolet-visible (UV-vis) spectroscopy, particle size analysis, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and high-resolution transmission electron microscopy (HRTEM) and then checked for their pro-oxidative (peroxidase and oxidase) activity. Furthermore, we studied the NZ kinetics and antibacterial properties of synthesized samples.

摘要

在本研究中,使用硝酸铈铵作为前驱体、碳酸铵作为沉淀剂,通过共沉淀法可靠地合成了促氧化铈纳米酶(CeO NZs)。通过改变沉淀剂的用量制备了不同的CeO NZs样品。采用紫外可见(UV-vis)光谱、粒度分析、X射线衍射(XRD)、X射线光电子能谱(XPS)和高分辨率透射电子显微镜(HRTEM)对合成的纳米酶进行了表征,然后检测了它们的促氧化(过氧化物酶和氧化酶)活性。此外,我们还研究了合成样品的纳米酶动力学和抗菌性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/45ef/11421543/04383618c161/d4na00234b-f1.jpg

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