Fang Pengkai, Wang Qingxu, Shen Xiaoqian, Zhao Jianyou, Wang Fan, Liu Zhong-Quan
Jiangsu Collaborative Innovation Center of Chinese Medicinal Resources Industrialization, College of Pharmacy, Nanjing University of Chinese Medicine, Nanjing 210023, China.
J Org Chem. 2024 Sep 6;89(17):12619-12627. doi: 10.1021/acs.joc.4c01548. Epub 2024 Aug 16.
An electrochemical synthesis of vinyl, alkyl, and allyl sulfones using sodium sulfinates and olefins was reported. This method uses direct current to pass through an undivided cell equipped with graphite carbon electrodes, and a series of diverse sulfone compounds can be synthesized at room temperature in high yields.
报道了一种使用亚磺酸钠和烯烃电化学合成乙烯基、烷基和烯丙基砜的方法。该方法利用直流电通过配备石墨碳电极的无隔膜电解槽，一系列不同的砜化合物可在室温下以高产率合成。
