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酸性介质对高填充可流动树脂基复合材料表面特性的影响:一项体外研究。

Effect of acidic media on surface characteristics of highly filled flowable resin-based composites: An in vitro study.

作者信息

Vulović Stefan, Blatz Markus B, Bukorović Jovan, Živković Nikola, Todorović Aleksandar, Vencl Aleksandar, Milić Lemić Aleksandra

机构信息

Department of Prosthodontics, School of Dental Medicine, University of Belgrade, Belgrade, Serbia.

Department of Preventive and Restorative Sciences, School of Dental Medicine, University of Pennsylvania, Philadelphia, Pennsylvania, USA.

出版信息

J Esthet Restor Dent. 2025 Feb;37(2):465-476. doi: 10.1111/jerd.13301. Epub 2024 Aug 20.

Abstract

OBJECTIVE

To analyze and compare the impact of acidic media on the surface characteristics of highly filled flowable resin-based composites.

MATERIALS AND METHODS

Two hundred fifty-six specimens were divided into four groups: GUF (G-aenial Universal Flo), GUI (G-aenial Universal Injectable), TEF (Tetric EvoFlow), and FSF (Filtek Supreme Flowable Restorative). Surface characteristics were analyzed before (T0) and after specimens immersion in different media, such as gastric juice (GJ), fizzy drink (FD), citric juice (CJ), or artificial saliva (AS), for 9 h (T1) and 18 h (T2). The analyses included surface roughness (SR) measurements, where average roughness (Ra) was obtained, scanning electron microscopy (SEM) analysis, and surface hardness (SH) evaluation, with Vickers numbers (HV) reported. The differences in values among groups/subgroups within the same stage were assessed using two-way ANOVA and Tukey's post hoc test, whereas repeated measures ANOVA with Bonferroni post hoc test was performed to compare the changes in values through the stages. Data were presented as mean ± standard deviation (SD).

RESULTS

At T0, GUI and GUF revealed lower Ra values (p < 0.05), more evenness in SEM micrographs, and higher HV values (p < 0.05) than FSF and TEF. At T1 and T2, specimens of all groups/subgroups demonstrated an increase in Ra and a decrease in HV compared with T0 (p < 0.05), as well as the changes in surface morphology on SEM micrographs. The lowest Ra and highest HV values were observed in GUI group, in contrast to FSF group, and in specimens immersed in GJ.

CONCLUSIONS

GUI revealed lower SR and higher SH compared to GUF and FSF both before and after exposure to acidic media. The presence of acidic media, especially GJ, significantly increases SR and decreases SH of tested materials.

CLINICAL SIGNIFICANCE

Information on the changes in the surface characteristics of highly filled resin-based composites after exposure to acidic media may be essential for the longevity of restorations like composite veneers fabricated from these materials.

摘要

目的

分析并比较酸性介质对高填料可流动树脂基复合材料表面特性的影响。

材料与方法

256个样本被分为四组:GUF(G-aenial通用流动树脂)、GUI(G-aenial通用可注射树脂)、TEF(Tetric EvoFlow)和FSF(Filtek Supreme可流动修复材料)。在样本浸入不同介质(如胃液(GJ)、汽水(FD)、柠檬汁(CJ)或人工唾液(AS))9小时(T1)和18小时(T2)之前(T0)和之后,分析其表面特性。分析包括表面粗糙度(SR)测量(获得平均粗糙度(Ra))、扫描电子显微镜(SEM)分析以及表面硬度(SH)评估,并报告维氏硬度值(HV)。同一阶段内各分组/亚组间数值的差异采用双向方差分析和Tukey事后检验进行评估,而采用重复测量方差分析和Bonferroni事后检验来比较各阶段数值的变化。数据以平均值±标准差(SD)表示。

结果

在T0时,与FSF和TEF相比,GUI和GUF的Ra值较低(p < 0.05),SEM显微照片更均匀,HV值较高(p < 0.05)。在T1和T2时,与T0相比,所有分组/亚组的样本Ra值增加,HV值降低(p < 0.05),并且SEM显微照片上的表面形态也发生了变化。与FSF组相比,GUI组以及浸入GJ的样本中观察到最低的Ra值和最高的HV值。

结论

与GUF和FSF相比,在暴露于酸性介质前后,GUI的SR较低,SH较高。酸性介质的存在,尤其是GJ,会显著增加测试材料的SR并降低其SH。

临床意义

暴露于酸性介质后高填料树脂基复合材料表面特性变化的信息对于由这些材料制成的复合贴面等修复体的使用寿命可能至关重要。

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