Spilmann J R
J Assoc Off Anal Chem. 1985 May-Jun;68(3):453-6.
A study was made to determine if the official AOAC method for screening of aflatoxin in corn could be modified for use as a quantitative method. Several different corn products were analyzed using the modified method, with an average savings of over 1 h/sample vs the CB method. Average recoveries for aflatoxin B1 were 94% for the low level spiked samples and 108% for the high level. Samples of corn and corn products containing naturally incurred aflatoxin were also analyzed with the modified method, and the results compared favorably with those obtained by the CB method.
开展了一项研究,以确定美国官方分析化学师协会(AOAC)用于玉米中黄曲霉毒素筛查的方法是否可以修改为定量方法。使用修改后的方法对几种不同的玉米产品进行了分析,与CB方法相比,每个样品平均节省了1个多小时。黄曲霉毒素B1在低水平加标样品中的平均回收率为94%,在高水平加标样品中的平均回收率为108%。还使用修改后的方法对含有天然存在黄曲霉毒素的玉米和玉米产品样品进行了分析,结果与CB方法获得的结果相比具有优势。