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基于气相色谱-质谱联用仪(GC-MS)和气相色谱-嗅闻仪(GC-O)揭示不同干燥方式下红茶香气的差异。

Revealing the differences in aroma of black tea under different drying methods based on GC-MS, GC-O.

作者信息

Lu Mingxia, Sheng Caiyan, Ke Han, Li Tiehan, Liu Qiuyan, Zhang Jixin, Li Luqing, Wang Yujie, Ning Jingming

机构信息

State Key Laboratory of Tea Plant Biology and Utilization, Anhui Agricultural University, 130 Changjiang West Road, Hefei 230036, China.

School of Tea and Food Science and Technology, Anhui Agricultural University, 130 Changjiang West Road, Hefei 230036, China.

出版信息

Food Chem X. 2024 Aug 26;23:101782. doi: 10.1016/j.fochx.2024.101782. eCollection 2024 Oct 30.

Abstract

Drying greatly affects the aroma of black tea. In this study, the differences in aroma of black tea under hot-air drying (HD), sun drying (SD), and pan-fired drying (PD) were investigated through quantitative descriptive analysis. Headspace solid-phase microextraction and solvent assisted flavor evaporation combined with gas chromatography-mass spectrometry and gas chromatography-olfactory were used to analyze the overall aroma profile of black tea. Aroma extract dilution analysis and odor activity values revealed that 15 aroma-active compounds led to differences in aroma, namely linalool, geraniol, phenylethyl alcohol, phenylacetaldehyde, () -linalool oxide (furanoid), -damascenone, dimethyl sulfide, methional, 2-methylbutanal, 3-methylbutanal, methyl salicylate, -myrcene, hexanal, 1-octen-3-ol, and heptanal. Among them, geraniol, linalool, and methional significantly enhanced the floral and roasty aroma of HD, while hexanal enhanced the green aroma of SD. Finally, our results were validated through aroma recombination and addition experiments. This study provides a theoretical basis for improving the aroma of black tea.

摘要

干燥对红茶香气有很大影响。本研究通过定量描述分析,研究了热风干燥(HD)、日晒干燥(SD)和锅炒干燥(PD)条件下红茶香气的差异。采用顶空固相微萃取和溶剂辅助风味蒸发结合气相色谱 - 质谱联用以及气相色谱 - 嗅觉分析法,分析红茶的整体香气特征。香气提取物稀释分析和气味活性值表明,15种香气活性化合物导致了香气差异,即芳樟醇、香叶醇、苯乙醇、苯乙醛、()-氧化芳樟醇(呋喃型)、β-大马酮、二甲基硫醚、甲硫醇、2-甲基丁醛、3-甲基丁醛、水杨酸甲酯、β-月桂烯、己醛、1-辛烯-3-醇和庚醛。其中,香叶醇、芳樟醇和甲硫醇显著增强了HD的花香和烘焙香气,而己醛增强了SD的青香。最后,通过香气重组和添加实验验证了我们的结果。本研究为改善红茶香气提供了理论依据。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/651e/11402106/00612d02443c/gr1.jpg

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