Duck B J, Woolias M
J Anal Toxicol. 1985 Jul-Aug;9(4):177-9. doi: 10.1093/jat/9.4.177.
A reversed-phase high performance liquid chromatographic (HPLC) method has been developed for the analysis of carbaryl in postmortem samples. It involves the use of an aqueous acetonitrile mobile phase to give rapid, reproducible analyses and an external standard for quantitation. Two separate extraction procedures (Extrelut column and protein precipitation with acetonitrile) are described; each one is suited to a particular substrate and each one leads to an almost complete recovery of carbaryl from that substrate.
已开发出一种反相高效液相色谱（HPLC）方法用于分析死后样本中的西维因。该方法使用乙腈水溶液作为流动相，以实现快速、可重复的分析，并采用外标法定量。文中描述了两种单独的提取程序（硅藻土柱法和乙腈蛋白沉淀法）；每种方法都适用于特定的底物，并且每种方法都能使西维因从该底物中几乎完全回收。
