• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

用于极端和受限环境的压电管堆叠式扫描隧道显微镜。

Piezo tube stacked scanning tunneling microscope for use in extreme and confined environments.

作者信息

Wang Jihao, Sun Mengbo

机构信息

High Magnetic Field Laboratory, Chinese Academy of Sciences, Hefei, Anhui 230031, China.

Department of General Education, Anhui Xinhua University, Hefei 230088, China.

出版信息

Micron. 2024 Dec;187:103719. doi: 10.1016/j.micron.2024.103719. Epub 2024 Sep 16.

DOI:10.1016/j.micron.2024.103719
PMID:39293141
Abstract

Scanning Tunneling Microscopy (STM) is widely used for observing atomic structures due to its ultra-high spatial resolution. As the core units of STM, the coarse stepper motor and imaging unit, have conflicting size requirements for piezo tubes. Longer piezo tubes yield greater output force and easier movement for the motor, while shorter tubes enhance imaging precision and stability for the scanner. Traditional STMs typically employ a large piezo tube for coarse stepping and a smaller one for independent imaging to address this issue. Here, we present the new design of a piezo tube stacked STM, in which two independent piezo tubes act together during tip-sample approach process and only one shorter tube works during scanning imaging. Both tubes are fixed to the framework, ensuring high rigidity and compactness. The new design enables us to achieve both coarse stepping and imaging functions with a total length of only 25 mm for the two tubes, effectively reducing the length of whole STM, facilitating its integration into narrow low-temperature spaces for imaging applications. Using this device, we obtained high-quality atomic images of graphite sample surfaces at room temperature. Continuous scanning imaging of the same area on Au film at 300 K demonstrates the STM's high stability in both X-Y and Z directions. Atomic images, I-V spectra, and di/dv spectra obtained at 2 K on graphite surface illustrate the excellent application potential of this device in low-temperature environments. Finally, atomic images obtained of graphite in sweeping the magnetic fields from 0 T to 11 T in a huge vibrational dry magnet prove the new STM's excellent performance in extreme conditions.

摘要

扫描隧道显微镜(STM)因其超高的空间分辨率而被广泛用于观察原子结构。作为STM的核心部件,粗调步进电机和成像单元对压电管的尺寸要求相互矛盾。较长的压电管能产生更大的输出力,使电机移动更轻松,而较短的压电管能提高扫描仪的成像精度和稳定性。传统的STM通常采用一个大的压电管进行粗调,一个较小的压电管进行独立成像来解决这个问题。在此,我们展示了一种压电管堆叠式STM的新设计,其中两个独立的压电管在针尖-样品接近过程中共同作用,而在扫描成像时只有一个较短的压电管工作。两个压电管都固定在框架上,确保了高刚性和紧凑性。这种新设计使我们能够在两根压电管总长度仅为25毫米的情况下实现粗调步进和成像功能,有效缩短了整个STM的长度,便于将其集成到狭窄的低温空间中用于成像应用。使用该设备,我们在室温下获得了石墨样品表面的高质量原子图像。在300 K下对金膜同一区域进行连续扫描成像,证明了STM在X-Y和Z方向上的高稳定性。在2 K下在石墨表面获得的原子图像、I-V谱和di/dv谱说明了该设备在低温环境中的优异应用潜力。最后,在一个巨大的振动干式磁体中从0 T到11 T扫描磁场时获得的石墨原子图像证明了这种新型STM在极端条件下的优异性能。

相似文献

1
Piezo tube stacked scanning tunneling microscope for use in extreme and confined environments.用于极端和受限环境的压电管堆叠式扫描隧道显微镜。
Micron. 2024 Dec;187:103719. doi: 10.1016/j.micron.2024.103719. Epub 2024 Sep 16.
2
Atomic imaging with a 12 T magnetic field perpendicular or parallel to the sample surface by an ultra-stable scanning tunneling microscope.采用超稳定扫描隧道显微镜在垂直或平行于样品表面的 12T 磁场中进行原子成像。
Ultramicroscopy. 2023 Sep;251:113774. doi: 10.1016/j.ultramic.2023.113774. Epub 2023 Jun 1.
3
A cryogen-free superconducting magnet based scanning tunneling microscope for liquid phase measurement.基于无液氦超导磁体的扫描隧道显微镜用于液相测量。
Rev Sci Instrum. 2023 Mar 1;94(3):033705. doi: 10.1063/5.0121761.
4
An ultracompact scanning tunneling microscope within a Φ 10 piezo tube in a 20 T superconducting magnet.一台置于20T超导磁体中、直径为10毫米的压电管内的超紧凑型扫描隧道显微镜。
Rev Sci Instrum. 2024 Mar 1;95(3). doi: 10.1063/5.0191662.
5
A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet.一种新型的能够在无液氦超导磁体中工作的原子分辨扫描隧道显微镜。
Micromachines (Basel). 2023 Mar 11;14(3):637. doi: 10.3390/mi14030637.
6
Atomically resolved low-temperature scanning tunneling microscope operating in a 22 T water-cooled magnet.在22T水冷磁体中运行的原子分辨率低温扫描隧道显微镜。
Ultramicroscopy. 2023 Mar;245:113668. doi: 10.1016/j.ultramic.2022.113668. Epub 2022 Dec 18.
7
Atomic-Resolution Imaging of Micron-Sized Samples Realized by High Magnetic Field Scanning Tunneling Microscopy.通过高磁场扫描隧道显微镜实现微米级样品的原子分辨率成像。
Micromachines (Basel). 2023 Jan 22;14(2):287. doi: 10.3390/mi14020287.
8
Isolated scan unit and scanning tunneling microscope for stable imaging in ultra-high magnetic fields.用于超高磁场中稳定成像的独立扫描单元和扫描隧道显微镜。
Ultramicroscopy. 2024 Jul;261:113960. doi: 10.1016/j.ultramic.2024.113960. Epub 2024 Mar 22.
9
Quick-connect scanning tunneling microscope head with nested piezoelectric coarse walkers.
Rev Sci Instrum. 2024 Jul 1;95(7). doi: 10.1063/5.0204940.
10
Atomic resolution imaging using a novel, compact and stiff scanning tunnelling microscope in cryogen-free superconducting magnet.在无低温超导磁体中使用新型、紧凑且坚固的扫描隧道显微镜进行原子分辨率成像。
J Microsc. 2024 Apr;294(1):26-35. doi: 10.1111/jmi.13262. Epub 2024 Jan 15.