Wang Jihao, Sun Mengbo
High Magnetic Field Laboratory, Chinese Academy of Sciences, Hefei, Anhui 230031, China.
Department of General Education, Anhui Xinhua University, Hefei 230088, China.
Micron. 2024 Dec;187:103719. doi: 10.1016/j.micron.2024.103719. Epub 2024 Sep 16.
Scanning Tunneling Microscopy (STM) is widely used for observing atomic structures due to its ultra-high spatial resolution. As the core units of STM, the coarse stepper motor and imaging unit, have conflicting size requirements for piezo tubes. Longer piezo tubes yield greater output force and easier movement for the motor, while shorter tubes enhance imaging precision and stability for the scanner. Traditional STMs typically employ a large piezo tube for coarse stepping and a smaller one for independent imaging to address this issue. Here, we present the new design of a piezo tube stacked STM, in which two independent piezo tubes act together during tip-sample approach process and only one shorter tube works during scanning imaging. Both tubes are fixed to the framework, ensuring high rigidity and compactness. The new design enables us to achieve both coarse stepping and imaging functions with a total length of only 25 mm for the two tubes, effectively reducing the length of whole STM, facilitating its integration into narrow low-temperature spaces for imaging applications. Using this device, we obtained high-quality atomic images of graphite sample surfaces at room temperature. Continuous scanning imaging of the same area on Au film at 300 K demonstrates the STM's high stability in both X-Y and Z directions. Atomic images, I-V spectra, and di/dv spectra obtained at 2 K on graphite surface illustrate the excellent application potential of this device in low-temperature environments. Finally, atomic images obtained of graphite in sweeping the magnetic fields from 0 T to 11 T in a huge vibrational dry magnet prove the new STM's excellent performance in extreme conditions.
扫描隧道显微镜(STM)因其超高的空间分辨率而被广泛用于观察原子结构。作为STM的核心部件,粗调步进电机和成像单元对压电管的尺寸要求相互矛盾。较长的压电管能产生更大的输出力,使电机移动更轻松,而较短的压电管能提高扫描仪的成像精度和稳定性。传统的STM通常采用一个大的压电管进行粗调,一个较小的压电管进行独立成像来解决这个问题。在此,我们展示了一种压电管堆叠式STM的新设计,其中两个独立的压电管在针尖-样品接近过程中共同作用,而在扫描成像时只有一个较短的压电管工作。两个压电管都固定在框架上,确保了高刚性和紧凑性。这种新设计使我们能够在两根压电管总长度仅为25毫米的情况下实现粗调步进和成像功能,有效缩短了整个STM的长度,便于将其集成到狭窄的低温空间中用于成像应用。使用该设备,我们在室温下获得了石墨样品表面的高质量原子图像。在300 K下对金膜同一区域进行连续扫描成像,证明了STM在X-Y和Z方向上的高稳定性。在2 K下在石墨表面获得的原子图像、I-V谱和di/dv谱说明了该设备在低温环境中的优异应用潜力。最后,在一个巨大的振动干式磁体中从0 T到11 T扫描磁场时获得的石墨原子图像证明了这种新型STM在极端条件下的优异性能。