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采用外标法23Na-qNMR对调味品、软饮料和矿泉水中钠浓度进行定量分析。

Quantitative analysis of sodium concentration in condiments, soft drinks, and mineral water by external standard 23Na-qNMR.

作者信息

Ogura Kenji

机构信息

Department of Food Science, Faculty of Bioresources and Environmental Sciences, Ishikawa Prefectural University, Nonoichi, Ishikawa, Japan.

出版信息

Biosci Biotechnol Biochem. 2024 Dec 23;89(1):88-94. doi: 10.1093/bbb/zbae150.

Abstract

Sodium is essential for human health, but excessive intake can lead to hypertension. Accurate sodium labeling in foods is critical due to increasing health awareness. This study investigated the use of 23Na nuclear magnetic resonance spectroscopy (NMR) for sodium quantification in condiments, soft drinks, and mineral water. In this study, external standard quantitative 23Na-NMR was used to measure sodium concentrations. Key steps included sample preparation, 90° pulse width calibration, and linewidth evaluation. The results showed that 23Na-NMR can accurately quantify sodium concentrations over a wide range, with good agreement with ion electrode methods. The results demonstrated that 23Na-NMR is a reliable method for the quantification of sodium in various liquid foods.

摘要

钠对人体健康至关重要,但过量摄入会导致高血压。由于健康意识的提高,食品中准确的钠标签至关重要。本研究调查了使用23Na核磁共振波谱法(NMR)对调味品、软饮料和矿泉水中的钠进行定量分析。在本研究中,采用外标定量23Na-NMR来测量钠浓度。关键步骤包括样品制备、90°脉冲宽度校准和线宽评估。结果表明,23Na-NMR能够在很宽的范围内准确地定量钠浓度,与离子电极法具有良好的一致性。结果表明,23Na-NMR是一种可靠的用于各种液态食品中钠定量分析的方法。

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