Li Jing, Shi Xiaoqin, Yang Kang, Guo Lang, Yang Junjie, Lan Zhengyu, Guo Yong, Xiao Longquan, Wang Xinhui
College of Food and Biological Engineering, Chengdu University, Chengdu 610106, PR China; College of Materials Science and Engineering, Sichuan University, Chengdu 610065, PR China.
College of Food and Biological Engineering, Chengdu University, Chengdu 610106, PR China.
Int J Biol Macromol. 2024 Dec;282(Pt 4):137114. doi: 10.1016/j.ijbiomac.2024.137114. Epub 2024 Oct 30.
In this study, carvacrol was effectively encapsulated in gelatin/chitosan composite nanofiber membrane using the electrospinning method with the help of the cationic surfactant cetyltrimethylammonium bromide (CTAB). The effects of CTAB (0.0%, 1.0%, w/w) and bioactive carvacrol (0.0%, 1.0%, 3.0%, 5.0%, 7.0%, 10.0%, w/w) on the structural, physicomechanical, antibacterial, and antioxidant characteristics of the nanofiber membranes were investigated. The results demonstrated that the antibacterial and antioxidant characteristics of the gelatin/chitosan composite nanofiber membrane (GC) and GC-CAR membrane (with the addition of 1.0% carvacrol) were unsatisfactory. As carvacrol and CTAB were both added, the elongation at break, antibacterial, and antioxidant properties of the nanofiber membranes significantly improved (p < 0.05), while the water vapor permeability (WVP) significantly decreased (p < 0.05). When the added amount of carvacrol was 5.0% (w/w), the nanofiber membrane (GC-CAR5-CTAB) exhibited the best antioxidant and antibacterial performance. Finally, the GC-CAR5-CTAB membrane was applied to the preservation of strawberries and Erjingtiao chilies, and their shelf life was effectively extended. The above results indicate that the nanofiber membrane prepared in this study has great potential for application in food-active packaging.
在本研究中,香芹酚在阳离子表面活性剂十六烷基三甲基溴化铵(CTAB)的辅助下,通过静电纺丝法有效地包封在明胶/壳聚糖复合纳米纤维膜中。研究了CTAB(0.0%、1.0%,w/w)和生物活性香芹酚(0.0%、1.0%、3.0%、5.0%、7.0%、10.0%,w/w)对纳米纤维膜的结构、物理机械性能、抗菌和抗氧化特性的影响。结果表明,明胶/壳聚糖复合纳米纤维膜(GC)和GC-CAR膜(添加1.0%香芹酚)的抗菌和抗氧化特性不理想。随着香芹酚和CTAB的同时添加,纳米纤维膜的断裂伸长率、抗菌和抗氧化性能显著提高(p<0.05),而水蒸气透过率(WVP)显著降低(p<0.05)。当香芹酚的添加量为5.0%(w/w)时,纳米纤维膜(GC-CAR5-CTAB)表现出最佳的抗氧化和抗菌性能。最后,将GC-CAR5-CTAB膜应用于草莓和二荆条辣椒的保鲜,有效延长了它们的货架期。上述结果表明,本研究制备的纳米纤维膜在食品活性包装方面具有巨大的应用潜力。