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超声辅助提取果壳纳米多糖的优化及其对光催化染料还原性能的评估与用于鲜切水果的可食用涂层研究

Optimization of ultrasonication assisted extraction of fruit shell nano polysaccharide and evaluation of photocatalytic dye reduction and edible coating for fresh-cut fruits.

作者信息

Sharma Madhu, Bains Aarti, Goksen Gulden, Ali Nemat, Khan Mohammad Rashid, Karabulut Gulsah, Chawla Prince

机构信息

Department of Food Technology and Nutrition, Lovely Professional University, Phagwara, Punjab 144411, India.

Department of Microbiology, Lovely Professional University, Phagwara, Punjab 144411, India.

出版信息

Food Chem X. 2024 Oct 15;24:101895. doi: 10.1016/j.fochx.2024.101895. eCollection 2024 Dec 30.

Abstract

(AM) fruit shell, considered waste, is an excellent source of bioactive compounds, including polysaccharides. Therefore, this study focuses on the extraction of AM polysaccharides using an ultrasonication-assisted approach. Different parameters, including ultrasonic power (200-600 W), time (5-15 min), and solid-to-solvent ratio (10-20 mg/mL), were employed, and significantly ( < 0.05) higher yield (16.93 %) was achieved at 400 W for 10 min. Monosaccharides composition revealed galactose (30.56 ± 0.76 %), galacturonic acid (24.72 ± 0.12 %), arabinose (17.26 ± 0.35 %), xylose (11.48 ± 0.21 %), glucose (10.52 ± 0.26 %), and rhamnose (5.39 ± 0.67 %), which were then confirmed by C spectrum. AM polysaccharides revealed nanoscale size with excellent structural crystallinity and thermal stability. Edible coatings of varying concentrations (0.5-2 %) were formulated and optimized 1 % coating, demonstrating efficacy in mitigating weight loss, microbial proliferation, and browning in cut apples. As well, AM polysaccharides prominently degraded 82.79 ± 0.39 % of methyl green. Overall, bael shells as a valuable source of polysaccharides, offering the potential for both photocatalytic dye degradation and food preservation.

摘要

(AM)果壳被视为废弃物,却是生物活性化合物(包括多糖)的优质来源。因此,本研究聚焦于采用超声辅助方法提取AM多糖。研究采用了不同参数,包括超声功率(200 - 600瓦)、时间(5 - 15分钟)和固液比(10 - 20毫克/毫升),结果显示在400瓦超声功率下处理10分钟时,多糖得率显著更高(<0.05),为16.93%。单糖组成分析显示含有半乳糖(30.56 ± 0.76%)、半乳糖醛酸(24.72 ± 0.12%)、阿拉伯糖(17.26 ± 0.35%)、木糖(11.48 ± 0.21%)、葡萄糖(10.52 ± 0.26%)和鼠李糖(5.39 ± 0.67%),随后通过碳谱得到证实。AM多糖呈现纳米级尺寸,具有优异的结构结晶度和热稳定性。制备了不同浓度(0.5 - 2%)的可食用涂层,并优化得到1%的涂层,该涂层在减轻切苹果的重量损失、抑制微生物增殖和防止褐变方面显示出效果。此外,AM多糖能显著降解82.79 ± 0.39%的甲基绿。总体而言,印度枳椇果壳是多糖的宝贵来源,在光催化染料降解和食品保鲜方面均具有潜力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/711d/11532754/1ae3271936b4/gr1.jpg

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