Ghorbani Z, Ehsani M H
Faculty of Physics, Semnan University, PO Box: 35195-363, Semnan, Iran.
Heliyon. 2024 Oct 11;10(20):e38869. doi: 10.1016/j.heliyon.2024.e38869. eCollection 2024 Oct 30.
Double perovskite BaFeMoO (BFMO) and doped with Ag ions were synthesized via the sol-gel method. The structural and antibacterial properties and viability of the samples were systematically investigated. The results of the Rietveld refinement indicated that both samples exhibited a single phase with cubic structure and space group Fm-3m. The substitution of Ag ions led to an increase in the unit cell and lattice parameters of BFMO, resulting in a change in the sample's morphology. The direct band gap (∼2eV) was measured for samples by Diffuse Reflectance Spectroscopy (DRS). Antibacterial activity of the BaFeMoO and BaAgFeMoO samples was assessed on the Gram-positive bacteria () and the Gram-negative bacteria () using the spread plate method. The results showed that the samples were effective against but not against . The sample doped with Ag ions showed a higher antibacterial effect than the pristine sample. An MTT assay of the normal fibroblast cell line treated with an Ag-doped sample showed a higher percentage of viability.
通过溶胶-凝胶法合成了双钙钛矿BaFeMoO(BFMO)及其掺杂Ag离子的样品。系统研究了样品的结构、抗菌性能和活力。Rietveld精修结果表明,两个样品均呈现具有立方结构和空间群Fm-3m的单相。Ag离子的取代导致BFMO的晶胞和晶格参数增加,从而使样品的形态发生变化。通过漫反射光谱(DRS)测量了样品的直接带隙(约2eV)。使用平板涂布法评估了BaFeMoO和BaAgFeMoO样品对革兰氏阳性菌()和革兰氏阴性菌()的抗菌活性。结果表明,样品对有效,但对无效。掺杂Ag离子的样品比原始样品显示出更高的抗菌效果。用掺杂Ag的样品处理的正常成纤维细胞系的MTT分析显示出更高的活力百分比。