An Analysis of the Influence of DSC Parameters on the Measurement of the Thermal Properties of Phase-Change Material.

A differential scanning calorimeter (DSC) is widely used for measuring the thermal properties of phase-change materials (PCMs). Optimizing test conditions based on material characteristics is essential for accurate results. This study investigates the effects of experimental parameters, including sample mass, heating rate, measurement modes, and atmosphere flow rate, on the phase-change enthalpy and phase-change temperature results. The findings indicate that variations in sample mass and heating rate lead to significant changes in phase-change temperatures, while an increase in purge gas flow rate reduces the phase-change enthalpy of the PCM. Based on the measurements, this study optimizes the DSC parameters and provides a reference for the accurate measurement of paraffin-based phase-change materials.