Eßer Marcus, Pratzer Marco, Frömming Marc, Duffhauß Jonas, Bhaskar Priyamvada, Krzyzowski Michael A, Morgenstern Markus
2nd Institute of Physics B and JARA-FIT, RWTH Aachen University, 52074 Aachen, Germany.
CryoVac GmbH and Co KG, 53842 Troisdorf, Germany.
Rev Sci Instrum. 2024 Dec 1;95(12). doi: 10.1063/5.0230892.
Low-temperature scanning tunneling spectroscopy is a key method to probe electronic and magnetic properties down to the atomic scale, but suffers from extreme vibrational sensitivity. This makes it challenging to employ closed-cycle cooling with its required pulse-type vibrational excitations, albeit this is mandatory to avoid helium losses for counteracting the continuously raising helium prices. Here, we describe a compact ultra-high vacuum scanning tunneling microscope (STM) system with an integrated primary pulse tube cooler (PTC) for closed-cycle operation. It achieves temperatures down to 1.5 K via a secondary Joule-Thomson stage and a z-noise down to 300 fmRMS in the STM junction for the frequency range of 0.1 Hz-5 kHz (feedback loop off). This is better than many STMs cooled by an external supply of liquid helium. The challenge to combine an effective vibrational decoupling from the PTC with sufficient thermal conduction is tackled by using a multipartite approach including the concept of bellows with minimal stiffness to decouple the PTC vibrationally from the STM and an optimized STM design with minimal vibrational transfer to the STM junction. As important benchmarks, we could reduce the voltage noise in the tunnel junction down to 120 μV and supply radio frequency excitations up to 40 GHz with amplitudes up to 10 mV in the junction via a close-by antenna. The development principally enables other secondary cooling stages such that it opens the perspective for a helium conserving operation of STMs across the whole interesting temperature range.
低温扫描隧道谱是探测直至原子尺度的电子和磁性质的关键方法,但它对振动极为敏感。这使得采用带有所需脉冲型振动激发的闭循环冷却具有挑战性,尽管为了抵消不断上涨的氦气价格所导致的氦气损失,这种冷却方式是必不可少的。在此,我们描述了一种紧凑型超高真空扫描隧道显微镜(STM)系统,该系统集成了用于闭循环运行的主脉冲管制冷机(PTC)。通过二级焦耳 - 汤姆逊级,它可实现低至1.5 K的温度,并且在STM结中,对于0.1 Hz - 5 kHz频率范围(反馈回路关闭),z噪声低至300 fmRMS。这比许多由外部供应液氦冷却的STM更好。通过采用包括具有最小刚度的波纹管概念以在振动上使PTC与STM解耦以及具有最小振动传递到STM结的优化STM设计在内的多部分方法,解决了将与PTC有效的振动解耦与足够的热传导相结合的挑战。作为重要的基准,我们能够将隧道结中的电压噪声降低至120 μV,并通过附近的天线在结中提供高达40 GHz的射频激励,幅度高达10 mV。该进展原则上允许使用其他二级冷却阶段,从而为STM在整个感兴趣的温度范围内的氦气节约运行开辟了前景。