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采用占位法制备的高孔隙率哈氏合金-X镍基高温合金的微观结构与力学性能

Microstructure and mechanical properties of highly porous Hastelloy-X nickel superalloy produced by a space holder approach.

作者信息

Bętkowska Aleksandra, Podsiadło Marcin, Polkowska Adelajda, Włoch Grzegorz, Polkowski Wojciech

机构信息

Łukasiewicz Research Network, Krakow Institute of Technology, Zakopiańska 73 Str, Krakow, 30-418, Poland.

Faculty of Non-Ferrous Metals, AGH University of Science and Technology, Mickiewicza 30 Av, Krakow, 30-059, Poland.

出版信息

Sci Rep. 2025 Jan 2;15(1):598. doi: 10.1038/s41598-024-84321-3.

DOI:10.1038/s41598-024-84321-3
PMID:39747266
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11697248/
Abstract

Highly porous nickel-based superalloys appear as attractive candidates to be applied e.g. as seals in gas turbine engines instead of honeycomb structures. Among various methods of producing open-porous materials, a space holder approach provides number of benefits regarding economic and ecological aspects of production. In this work, the pioneering results of microstructure and mechanical properties analyses of highly porous Hastelloy-X nickel superalloy produced by the space holder approach, are presented. The materials were fabricated by using spherical fine Hastelloy-X powders and carbamide particles as batch materials. A multi-step powder metallurgy and thermomechanical processing was applied to produce open porous samples having a total volumetric porosity of 50, 60 and 70%. The produced materials were subjected to non-destructive (X-ray computed tomography) and metallographic inspections. Mechanical properties of the porous Hastelloy-X samples were examined in static room temperature compression tests, to discuss the effect of obtained porosity on compressive response.

摘要

高度多孔的镍基高温合金似乎是有吸引力的候选材料,例如可用于燃气涡轮发动机的密封件,以替代蜂窝结构。在各种生产开孔材料的方法中,占位法在生产的经济和生态方面具有诸多优势。在这项工作中,展示了通过占位法生产的高度多孔哈氏合金X镍基高温合金的微观结构和力学性能分析的开创性成果。这些材料是通过使用球形细哈氏合金X粉末和尿素颗粒作为批料制造的。采用多步粉末冶金和热机械加工来生产总体积孔隙率为50%、60%和70%的开孔多孔样品。对所生产的材料进行了无损(X射线计算机断层扫描)和金相检查。在静态室温压缩试验中检查了多孔哈氏合金X样品的力学性能,以讨论所得孔隙率对压缩响应的影响。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/dcf4216d74a0/41598_2024_84321_Fig8_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/aa6779e217c6/41598_2024_84321_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/24582fafb6cb/41598_2024_84321_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/93d8bdb5e943/41598_2024_84321_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/1c18bd49172f/41598_2024_84321_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/79878e4816ec/41598_2024_84321_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/c0a32c5772ae/41598_2024_84321_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/29eeaa7ae89f/41598_2024_84321_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/dcf4216d74a0/41598_2024_84321_Fig8_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/aa6779e217c6/41598_2024_84321_Fig1_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/24582fafb6cb/41598_2024_84321_Fig2_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/93d8bdb5e943/41598_2024_84321_Fig3_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/1c18bd49172f/41598_2024_84321_Fig4_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/79878e4816ec/41598_2024_84321_Fig5_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/c0a32c5772ae/41598_2024_84321_Fig6_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/29eeaa7ae89f/41598_2024_84321_Fig7_HTML.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a2d5/11697248/dcf4216d74a0/41598_2024_84321_Fig8_HTML.jpg

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本文引用的文献

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ACS Omega. 2022 Jan 27;7(5):4202-4213. doi: 10.1021/acsomega.1c05841. eCollection 2022 Feb 8.
2
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Materials (Basel). 2019 Feb 5;12(3):486. doi: 10.3390/ma12030486.