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基于响应面法的陶瓷玻璃地质聚合物砂浆配合比设计与性能的试验研究

Experimental studies on mix design and properties of ceramic-glass geopolymer mortars using response surface methodology.

作者信息

Pourabbas Bilondi Meysam, Ghaffarian Vahideh, Amiri Daluee Mahdi, Pakizehrooh Reyhaneh, Hosseini Tazik Saeed, Behzadian Alireza, Zaresefat Mojtaba

机构信息

Department of Civil Engineering, University of Gonabad, Gonabad, Iran.

Faculty of Civil Engineering and Environment, Khavaran Institute of Higher Education, Mashhad, Iran.

出版信息

Sci Rep. 2025 Jan 2;15(1):282. doi: 10.1038/s41598-024-82658-3.

Abstract

This study explores the mechanical properties of geopolymer mortars incorporating ceramic and glass powders sourced from industrial waste. A Box-Behnken design was employed to assess the effects of ceramic waste powder (CWP) content, alkaline activator ratio, solution-to-binder (S: B) ratio, and oven curing duration on the mortar's performance. Compressive strengths were measured at 3 and 28 days, and regression models were developed to predict these outcomes. The relationships between compressive strength, flexural strength, and ultrasonic pulse velocity (UPV) were also analyzed. Microstructural and molecular changes were investigated using scanning electron microscopy and fourier transform infrared spectroscopy. According to response surface methodology results, the maximum compressive strengths of 22.79 MPa at three days and 25 MPa at 28 days were achieved using a mix containing 85.8% CWP, a 1.02 sodium hydroxide (NH): sodium silicate (NS) ratio, a 0.647 S: B ratio, and a 12-h oven curing time. Optimal oven curing conditions resulted in 28-day compressive strength, flexural strength, and UPV values of 25.7 MPa, 5.62 MPa, and 5765 m/s, respectively..

摘要

本研究探讨了掺入源自工业废料的陶瓷和玻璃粉末的地质聚合物砂浆的力学性能。采用Box-Behnken设计来评估陶瓷废料粉末(CWP)含量、碱性活化剂比例、溶液与粘结剂(S:B)比例以及烘箱养护时间对砂浆性能的影响。在3天和28天时测量抗压强度,并建立回归模型来预测这些结果。还分析了抗压强度、抗折强度和超声波脉冲速度(UPV)之间的关系。使用扫描电子显微镜和傅里叶变换红外光谱研究微观结构和分子变化。根据响应面法结果,使用含有85.8% CWP、氢氧化钠(NH)与硅酸钠(NS)比例为1.02、S:B比例为0.647且烘箱养护时间为12小时的混合物,在3天时获得了22.79 MPa的最大抗压强度,在28天时获得了25 MPa的最大抗压强度。最佳烘箱养护条件下,28天的抗压强度、抗折强度和UPV值分别为25.7 MPa、5.62 MPa和5765 m/s。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f0c7/11696182/7e1231956864/41598_2024_82658_Fig1_HTML.jpg

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