Li Huayu, Yan Shaohui, Xu Hongtao, Li Xiaoyu, Wang Runan, Yan Ying, Li Pengyu, Zhang Litao, Wang Yanqing, Zu Mengmeng, Wang Yibo
Key Laboratory for Standardization of Reconstituted Tobacco Sheet in the Tobacco Industry, Henan Provincial Engineering Research Center for Reconstituted Tobacco Sheet, Henan Cigarette Industrial Reconstituted Tobacco Sheet Co., Ltd., Xuchang, 461000, People's Republic of China.
Luo he Vocational Technology College, Luohe, 462000, People's Republic of China.
Sci Rep. 2025 Jan 9;15(1):1539. doi: 10.1038/s41598-025-85562-6.
In order to study the change rule of freshness and acid ions in reconstituted tobacco slurry, the content changes of 17 organic acids and 5 inorganic anions in reconstituted tobacco slurry with different residence times under confined condition were determined by on-line solid-phase extraction ion chromatography in this study. The results showed that the changes of acetic acid, nitrate ion and isovaleric acid in different reconstituted tobacco slurries with oscillation time were regular and consistent, and the trends of the changes of acetic acid, nitrate ion and isovaleric acid in different reconstituted tobacco slurries with oscillation time were correlated with each other in a highly significant way. Taking the evaluation of olfactory aroma and sensory quality qualities of reconstituted tobacco pulps with different residence times as a benchmark, it was found that the variation patterns of nitrate ions and isovaleric acid in reconstituted tobacco pulps with oscillation time were consistent with the variation patterns of olfactory and sensory qualities in the process of closed oscillation; compared with the fresh pulp, the olfactory aroma and sensory qualities of tobacco pulps had unpleasant odours appearing when the content of nitrate ions was reduced by about 48%. The selection of isovaleric acid and nitrate ion as the characteristic components of tobacco reconstituted pulp for monitoring can provide technology for optimising pulp retention time and production process.
为研究再造烟叶浆料中鲜度及酸离子的变化规律,本研究采用在线固相萃取离子色谱法测定了密闭条件下不同停留时间的再造烟叶浆料中17种有机酸和5种无机阴离子的含量变化。结果表明,不同再造烟叶浆料中乙酸、硝酸根离子和异戊酸随振荡时间的变化规律一致,且不同再造烟叶浆料中乙酸、硝酸根离子和异戊酸随振荡时间的变化趋势高度显著相关。以不同停留时间的再造烟叶浆的嗅觉香气和感官品质评价为基准,发现再造烟叶浆中硝酸根离子和异戊酸随振荡时间的变化规律与密闭振荡过程中嗅觉和感官品质的变化规律一致;与新鲜浆相比,当硝酸根离子含量降低约48%时,烟叶浆的嗅觉香气和感官品质出现不愉快气味。选择异戊酸和硝酸根离子作为监测再造烟叶浆的特征成分,可为优化浆料停留时间和生产工艺提供技术支持。