Simpson R M, Suhre F B, Shafer J W
J Assoc Off Anal Chem. 1985 Jan-Feb;68(1):23-6.
A gas chromatographic-mass spectrometric procedure using isotopically labeled internal standards and the technique of selective-ion monitoring was used to assay sulfamethazine, sulfadimethoxine, sulfabromethazine, sulfathiazole, and sulfaquinoxaline in liver and muscle tissue of swine, poultry, and cattle. The data presented clearly demonstrate the applicability of this procedure for confirmation of sulfonamide residues in animal tissue.
采用气相色谱-质谱联用方法，使用同位素标记内标和选择性离子监测技术，对猪、家禽和牛的肝脏及肌肉组织中的磺胺二甲嘧啶、磺胺地索辛、磺胺溴甲嘧啶、磺胺噻唑和磺胺喹恶啉进行测定。所呈现的数据清楚地证明了该方法在确认动物组织中磺胺类药物残留方面的适用性。
