Khazaei Mohammad, Dehvedar Mohsen
Petroleum Department, AmirKabir University of Technology, Tehran, Iran.
Heliyon. 2025 Feb 14;11(4):e42699. doi: 10.1016/j.heliyon.2025.e42699. eCollection 2025 Feb 28.
Fluid loss changes the slurry's rheological and mechanical properties. Thus, fluid loss proves that the slurry cannot have proper properties. This study tests several types of FLC (fluid loss control) and a liquid dispersant on fresh cement slurries. The study examined changes in several properties. These include rheological properties, compressive strength, fluid loss control, free water, settling, mixing, and thickening time. Also, fluid migration from the pumped cement is a big issue during well cementing. Excessive fluid loss can allow gas to enter the cement slurry. So, fluid loss control additives are used to reduce gas migration. The cement slurry weight was 118 pcf used in 13 3/8″ casing and 7″ liners. Materials with different functional groups were tested: amide, ester, ether, alcohol, and carboxylic acid. Finally, an FLC was made by combining two substances. They had ester and ether functional groups. The Final decision was to mix three substances. They were FLC1, FLC2, and a liquid dispersant. To control the properties of a fresh cement slurry. The target values were 180 and 210 °F for compressive strength and 150 and 180 °F for BHCT. The designed formulation using these additives leads to a reduction in transition time. Reducing transition time helps cut gas migration into the cement slurry.
滤失会改变水泥浆的流变学和力学性能。因此,滤失表明水泥浆无法具备合适的性能。本研究对几种类型的滤失控制剂(FLC)和一种液体分散剂在新鲜水泥浆上进行了测试。该研究考察了几种性能的变化。这些性能包括流变性能、抗压强度、滤失控制、自由水、沉降、混合以及稠化时间。此外,在固井过程中,从泵送水泥中发生的流体迁移是一个大问题。过度滤失会使气体进入水泥浆。所以,使用滤失控制添加剂来减少气体迁移。在13 3/8英寸套管和7英寸尾管中使用的水泥浆密度为118磅/立方英尺。对具有不同官能团的材料进行了测试:酰胺、酯、醚、醇和羧酸。最后,通过将两种物质组合制成了一种滤失控制剂。它们具有酯和醚官能团。最终决定混合三种物质。它们是FLC1、FLC2和一种液体分散剂。以控制新鲜水泥浆的性能。抗压强度的目标值为180和210°F,井底循环温度(BHCT)的目标值为150和180°F。使用这些添加剂设计的配方可缩短过渡时间。缩短过渡时间有助于减少气体向水泥浆中的迁移。