Bender Philipp, Leliaert Jonathan, Bersweiler Mathias, Honecker Dirk, Michels Andreas
Department of Physics and Materials Science University of Luxembourg 162A Avenue de la Faïencerie L-1511 Luxembourg Grand Duchy of Luxembourg.
Department of Solid State Sciences Ghent University Krijgslaan 281/S1 9000 Ghent Belgium.
Small Sci. 2020 Sep 6;1(1):2000003. doi: 10.1002/smsc.202000003. eCollection 2021 Jan.
One of the key challenges in magnetism remains the determination of the nanoscopic magnetization profile within the volume of thick samples, such as permanent ferromagnets. Thanks to the large penetration depth of neutrons, magnetic small-angle neutron scattering (SANS) is a powerful technique to characterize bulk samples. The major challenge regarding magnetic SANS is accessing the real-space magnetization vector field from the reciprocal scattering data. In this study, a fast iterative algorithm is introduced that allows one to extract the underlying 2D magnetic correlation functions from the scattering patterns. This approach is used here to analyze the magnetic microstructure of Nanoperm, a nanocrystalline alloy which is widely used in power electronics due to its extraordinary soft magnetic properties. It can be shown that the computed correlation functions clearly reflect the projection of the 3D magnetization vector field onto the detector plane, which demonstrates that the used methodology can be applied to probe directly spin textures within bulk samples with nanometer resolution.
磁学领域的关键挑战之一仍是确定厚样品(如永磁体)内部的纳米级磁化分布。由于中子的穿透深度大,磁小角中子散射(SANS)是表征块状样品的一种强大技术。磁SANS面临的主要挑战是从倒易散射数据中获取实空间磁化矢量场。在本研究中,引入了一种快速迭代算法,该算法能够从散射图案中提取潜在的二维磁相关函数。此方法在此用于分析纳米晶合金纳米坡莫合金的磁微结构,该合金因其优异的软磁性能而广泛应用于电力电子领域。可以证明,计算得到的相关函数清楚地反映了三维磁化矢量场在探测器平面上的投影,这表明所使用的方法可应用于以纳米分辨率直接探测块状样品内的自旋纹理。