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正畸托槽在模拟胃酸和唾液中的腐蚀、表面粗糙度及离子释放分析。

Analysis of corrosion, surface roughness, and ıon release of orthodontic brackets in simulated gastric acid and saliva.

作者信息

Umurca Dilara Gülhan, Sasany Rafat, Gülyurt Muzaffer

机构信息

Department of Othodontics, Faculty of Dentistry, Biruni University, İstanbul, Turkey.

Department of Prosthodontics, Faculty of Dentistry, Biruni University, İstanbul, Turkey.

出版信息

Sci Rep. 2025 Apr 29;15(1):14984. doi: 10.1038/s41598-025-93039-9.

Abstract

This study aims to assess the ion release (Ni, Cr) and surface roughness of metal (M), self-ligating (SL), and ceramic (C) orthodontic brackets after exposure to simulated gastric acid (pH 1.5, pH 3.0) and artificial saliva (pH 7.0). A total of 198 brackets, metal brackets (M) (n = 66) self-ligating (SL) (n = 66), and ceramic brackets (C) (n = 66) were used in this study. Gastric solutions mimicking human gastroesophageal reflux with a pH of 1, 5 or 3 and as a control group pH of 7 (artificial saliva) were used. All specimens were immersed in test solutions for 30 min, 24 h, and 1 month (n = 22 per group). Inductively coupled plasma-mass spectrometry (ICP-MS) measured ion release, while an optical profilometer assessed surface roughness. Data were analyzed using One-way ANOVA and t-tests (p < 0.05). Ni and Cr ion release peaked at 24 h and decreased by 1 month (p < 0.05). SL brackets released the most ions, particularly in acidic conditions (p < 0.05). Surface roughness was highest at 24 h, then decreased (p < 0.001), with M brackets showing the greatest roughness and C brackets the lowest (p < 0.001). M and SL brackets had the highest roughness at pH 1.5, while C brackets peaked at pH 3.0 (p < 0.001). Acidic conditions significantly impact ion release and surface roughness. Ceramic brackets may be advantageous for patients with reflux disease, offering reduced corrosion and surface alterations.

摘要

本研究旨在评估金属(M)、自结扎(SL)和陶瓷(C)正畸托槽在暴露于模拟胃酸(pH 1.5、pH 3.0)和人工唾液(pH 7.0)后的离子释放(镍、铬)和表面粗糙度。本研究共使用了198个托槽,其中金属托槽(M)(n = 66)、自结扎托槽(SL)(n = 66)和陶瓷托槽(C)(n = 66)。使用模拟人类胃食管反流且pH值为1、5或3的胃液以及pH值为7的对照组(人工唾液)。所有标本在测试溶液中浸泡30分钟、24小时和1个月(每组n = 22)。电感耦合等离子体质谱法(ICP-MS)测量离子释放,而光学轮廓仪评估表面粗糙度。数据采用单因素方差分析和t检验进行分析(p < 0.05)。镍和铬离子释放在24小时达到峰值,并在1个月时下降(p < 0.05)。SL托槽释放的离子最多,尤其是在酸性条件下(p < 0.05)。表面粗糙度在24小时时最高,然后下降(p < 0.001),M托槽的粗糙度最大,C托槽的粗糙度最小(p < 0.001)。M和SL托槽在pH 1.5时粗糙度最高,而C托槽在pH 3.0时达到峰值(p < 0.001)。酸性条件会显著影响离子释放和表面粗糙度。陶瓷托槽对患有反流疾病的患者可能具有优势,可减少腐蚀和表面变化。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e6f8/12041320/d445fd20a63a/41598_2025_93039_Fig1_HTML.jpg

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