Kilponen Leeni, Varrela Juha, Vallittu Pekka K
Institute of Dentistry, University of Turku, Turku, Finland.
Division of Welfare, Turku, Finland.
Biomater Investig Dent. 2019 Nov 6;6(1):61-72. doi: 10.1080/26415275.2019.1684823. eCollection 2019.
To investigate if primers can be used to modify bonding characteristics of orthodontic brackets. Stainless steel, zirconia-alumina ceramic and polycarbonate brackets were bonded to enamel with and without universal and bracket material specific primers on the bracket base. Orthodontic adhesive cement (Transbond™XT) was used for bonding. The primers in each group ( = 10) were silane based (RelyX™ Ceramic Primer) and universal primer (Monobond Plus) for ceramic and metal brackets, and adhesive resin (Adper™ Scotchbond™ Multi-Purpose Adhesive) and composite primer (GC Composite Primer) for polycarbonate brackets. Controls with no primer were used for all bracket types. Teeth with bonded brackets were stored in distilled water in 37 °C for 7 days and debonded with static shear loading. Debonding forces were recorded and analyzed with ANOVA. Adhesive remnant index (ARI) was determined and enamel damage examined. The bond strength without primers was 8.14 MPa (±1.49) for metal, 21.9 MPa (±3.55) for ceramic and 10.47 MPa (±2.11) for polycarbonate brackets ( < .05). Using silane as primer increased the bond strength of ceramic brackets significantly to 26.45 MPa (±5.00) ( < .05). ARI-scores were mostly 2-3 (>50% of the adhesive left on the enamel after debonding), except with silane and ceramic brackets, ARI-score was mostly 0-1 (>50% of the adhesive left on the bracket). Debonding caused fractured enamel in four specimens with ceramic brackets. Bond strength was highest for ceramic brackets. Silane primer increased bond strength when used with ceramic brackets leading to enamel fractures, but otherwise primers had only minor effect on the bond strength values.
为研究引物是否可用于改变正畸托槽的粘结特性。将不锈钢、氧化锆-氧化铝陶瓷和聚碳酸酯托槽在有无通用型及托槽材料专用引物的情况下粘结于牙釉质表面,引物涂覆于托槽基底。使用正畸粘结水门汀(Transbond™XT)进行粘结。每组(n = 10)中,用于陶瓷和金属托槽的引物为硅烷类(RelyX™ Ceramic Primer)和通用引物(Monobond Plus),用于聚碳酸酯托槽的引物为粘结树脂(Adper™ Scotchbond™ Multi-Purpose Adhesive)和复合引物(GC Composite Primer)。所有托槽类型均设置无引物对照组。将粘结有托槽的牙齿在37℃蒸馏水中保存7天,然后通过静态剪切加载进行脱粘。记录脱粘力并用方差分析进行分析。测定粘结残留指数(ARI)并检查牙釉质损伤情况。无引物时,金属托槽的粘结强度为8.14MPa(±1.49),陶瓷托槽为21.9MPa(±3.55),聚碳酸酯托槽为10.47MPa(±2.11)(P < 0.05)。使用硅烷作为引物可使陶瓷托槽的粘结强度显著提高至26.45MPa(±5.00)(P <