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采用顶空-气相色谱-离子迁移谱(HS-GC-IMS)和顶空固相微萃取-气相色谱-质谱联用(HS-SPME-GC-MS)对汤在烹饪过程中的香气成分进行综合表征与比较

Comprehensive Characterization and Comparison of Aroma Profiles of Soup During the Cooking Process by HS-GC-IMS and HS-SPME-GC-MS.

作者信息

Yan Ni-Na, Xu Cheng-Jian, Xiong Shuang-Li, Li Xiang, Gu Si-Yu, Zhu Zhong-Yan, Liu Yang, Zhu Nan, Zhou Yu, Xiao Hang

机构信息

Key Laboratory of Sichuan Cuisine Artificial Intelligence, Sichuan Tourism University, Chengdu 610100, China.

College of Culinary and Food Science Engineering, Sichuan Tourism University, Chengdu 610100, China.

出版信息

Foods. 2025 Apr 24;14(9):1478. doi: 10.3390/foods14091478.

Abstract

Many scholars have studied soup, but there are relatively few studies exploring the aroma changes during its cooking process using different detection methods. The aroma of soup was analyzed and compared using electronic nose (E-nose) analysis, headspace gas chromatography-ion mobility spectrometry (HS-GC-IMS), and headspace-solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS). A significant effect of cooking time on the overall aroma profile of soup was identified through E-nose analysis. By HS-GC-IMS and HS-SPME-GC-MS analysis, 51 volatile aroma compounds were detected, with alcohols and aldehydes identified as the main aroma substances. Based on the relative odor activity value (ROAV) and multivariate statistical analysis, 1-octen-3-ol, 1-octanol, methyl cinnamate, and 2-pentyl furan were determined to be the key aroma compounds in the cooking process. We observed that shorter cooking time preserved the mushroom aroma of soup most effectively. These findings can be utilized for the industrial production of soup and for optimization of its key aroma components.

摘要

许多学者都对[汤品名称]进行过研究,但运用不同检测方法探究其烹饪过程中香气变化的研究相对较少。采用电子鼻(E-nose)分析、顶空气相色谱-离子迁移谱(HS-GC-IMS)以及顶空固相微萃取-气相色谱-质谱联用(HS-SPME-GC-MS)对[汤品名称]的香气进行了分析和比较。通过电子鼻分析确定了烹饪时间对[汤品名称]整体香气特征有显著影响。通过HS-GC-IMS和HS-SPME-GC-MS分析,检测出51种挥发性香气化合物,其中醇类和醛类被确定为主要香气物质。基于相对气味活性值(ROAV)和多元统计分析,确定1-辛烯-3-醇、1-辛醇、肉桂酸甲酯和2-戊基呋喃为烹饪过程中的关键香气化合物。我们观察到较短的烹饪时间能最有效地保留[汤品名称]的蘑菇香气。这些研究结果可用于[汤品名称]的工业化生产及其关键香气成分的优化。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f1fa/12071240/3625835be72e/foods-14-01478-g001.jpg

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