Abdullah Kamran Muhammad
Department of Pedodontics and Orthodontic Sciences, College of Dentistry, King Khalid University, Abha, Saudi Arabia.
Korean J Orthod. 2025 Jul 25;55(4):244-253. doi: 10.4041/kjod24.246. Epub 2025 May 14.
Effects of contemporary remineralization agents on the repair and regeneration of eroded enamel, specifically examining Vickers hardness (VH), shear bond strength (SBS), the calcium/phosphorus (Ca/P) ratio, and bracket-enamel interface.
Extracted maxillary premolars with intact enamel were selected. Sixteen samples with sound uneroded enamel (Group 1, control) and eighty artificially eroded samples were used. The eroded samples (n = 80) were etched with phosphoric acid and divided into five remineralization treatment groups (Groups 2, 3, 4, 5, and 6) based on the type of remineralization applied. VH and Ca/P ratios were assessed using energy dispersive X-ray spectroscopy. All samples were primed and bonded with orthodontic brackets. Two samples from each group were assessed under a scanning electron microscope to analyze the bracket-enamel interface. The remaining samples underwent SBS testing. The debonded surfaces were evaluated using the adhesive remnant index. Statistical analysis was conducted using ANOVA and post hoc multiple comparison tests ( < 0.05).
The lowest SBS was recorded in Group 2, where brackets were bonded to eroded enamel. In contrast, the highest SBS was observed in sound enamel. Group 2 also exhibited the lowest Ca/P ratio, while sound enamel demonstrated the highest mean VH. Notably, eroded enamel treated with hydroxyapatite nanoparticles (HAnp), NR-5, and Curodont Repair exhibited VH comparable to sound enamel.
Eroded enamel remineralized with HAnp, NR-5, and Curodont Repair demonstrated improved VH and SBS when metallic brackets were bonded to the enamel surface, suggesting potential effectiveness in orthodontic applications.
研究当代再矿化剂对侵蚀性牙釉质修复和再生的影响,具体检测维氏硬度(VH)、剪切粘结强度(SBS)、钙/磷(Ca/P)比以及托槽-牙釉质界面。
选取牙釉质完整的上颌前磨牙。使用16个牙釉质未受侵蚀的样本(第1组,对照组)和80个人工侵蚀样本。将侵蚀样本(n = 80)用磷酸酸蚀,并根据所应用的再矿化类型分为五个再矿化治疗组(第2、3、4、5和6组)。使用能量色散X射线光谱法评估VH和Ca/P比。所有样本均进行预处理并粘结正畸托槽。每组取两个样本在扫描电子显微镜下进行评估,以分析托槽-牙釉质界面。其余样本进行SBS测试。使用粘结剂残留指数评估脱粘表面。采用方差分析和事后多重比较检验进行统计分析(< 0.05)。
第2组中托槽粘结于侵蚀性牙釉质,其SBS最低。相比之下,在完好牙釉质中观察到最高的SBS。第2组的Ca/P比也最低,而完好牙釉质的平均VH最高。值得注意的是,用羟基磷灰石纳米颗粒(HAnp)、NR-5和Curodont Repair处理的侵蚀性牙釉质,其VH与完好牙釉质相当。
当金属托槽粘结于牙釉质表面时,用HAnp、NR-5和Curodont Repair再矿化的侵蚀性牙釉质表现出改善的VH和SBS,表明在正畸应用中具有潜在效果。