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蔓越莓增强聚甲基丙烯酸甲酯义齿基托树脂的弯曲强度、冲击强度和表面显微硬度的体外评价

In Vitro Evaluation of Flexural Strength, Impact Strength, and Surface Microhardness of Vaccinium macrocarpon Reinforced Polymethyl Methacrylate Denture Base Resin.

作者信息

Viswanathan Anitha Kuttae, Krishnan Rajkumar

机构信息

Department of Prosthodontics, SRM Dental College, Chennai, Tamil Nadu, India.

Department of Oral Pathology, SRM Dental College, Chennai, Tamil Nadu, India.

出版信息

Clin Exp Dent Res. 2025 Jun;11(3):e70145. doi: 10.1002/cre2.70145.

Abstract

OBJECTIVE

The antimicrobial efficacy of cranberry (CA) against oral infections was well evidenced. Influence of cranberry on the mechanical properties of heat-activated polymethyl methacrylate (HA-PMMA) denture base resin (DBR) is unexplored till date and is significant for a better understanding of the reinforcement. This study aimed to evaluate the flexural strength (FS), impact strength (IS), and surface microhardness (VHN) of heat-cure PMMA DBR reinforced with varying concentrations of Vaccinium macrocarpon (cranberry) extract.

MATERIAL AND METHODS

A total of 150 samples were categorized into five groups (n = 10) by weight percentage of 0, 0.5, 1.0, 1.5, and 2.0 cranberry extract added into HA-PMMA polymer after the performance of antimicrobial efficacy testing of CA. Three-point bending test for FT, Izod impact testing for IS, and Vickers microhardness test were performed. Fractured sample surface was characterized by a high-resolution scanning electron microscope (HR-SEM). Raw data were statistically analyzed with one-way ANOVA and post hoc Bonferroni test.

RESULTS

A significant improvement in flexural strength of 76.88 ± 0.73 MPa, impact strength of 6.66 ± 0.24 kJ/m, and microhardness of 18.44 ± 0.27 kg/mm was observed at 2 wt.% (p < 0.0001). Fractured surface topography showed dispersion of cranberry particles as a thin fibrous band intermeshed within resin matrix.

CONCLUSIONS

Addition of up to 2 wt.% cranberry improved the FS, IS, and VHN on comparison to 0 wt.% control HA-PMMA.

摘要

目的

蔓越莓(CA)对口腔感染的抗菌效果已有充分证据。蔓越莓对热活化聚甲基丙烯酸甲酯(HA-PMMA)义齿基托树脂(DBR)力学性能的影响至今尚未探索,这对于更好地理解增强作用具有重要意义。本研究旨在评估用不同浓度的大果越桔(蔓越莓)提取物增强的热固化PMMA DBR的弯曲强度(FS)、冲击强度(IS)和表面显微硬度(VHN)。

材料与方法

在对CA进行抗菌效果测试后,将150个样品按添加到HA-PMMA聚合物中的蔓越莓提取物重量百分比分为五组(n = 10),分别为0%、0.5%、1.0%、1.5%和2.0%。进行了FT的三点弯曲试验、IS的悬臂梁冲击试验和维氏显微硬度试验。用高分辨率扫描电子显微镜(HR-SEM)对断裂样品表面进行表征。原始数据采用单因素方差分析和事后Bonferroni检验进行统计分析。

结果

在2 wt.%时,观察到弯曲强度显著提高至76.88 ± 0.73 MPa,冲击强度提高至6.66 ± 0.24 kJ/m,显微硬度提高至18.44 ± 0.27 kg/mm(p < 0.0001)。断裂表面形貌显示蔓越莓颗粒分散为交织在树脂基质中的细纤维带。

结论

与0 wt.%的对照HA-PMMA相比,添加高达2 wt.%的蔓越莓可改善FS、IS和VHN。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/441f/12086990/2b63431fb1d9/CRE2-11-e70145-g001.jpg

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