Zhang Bo, Zhang Ji, Le Qiaoli, Wang Duoduo, Ding Jiangtao, Xu Chaohua
School of Civil Engineering and Architecture, Guizhou Minzu University, Guiyang 550025, China.
Materials (Basel). 2025 May 26;18(11):2491. doi: 10.3390/ma18112491.
Modified phosphogypsum (MPG) is a new type of solid waste, which could show unique mechanical properties in complex stress conditions. In this study, the effects of different loading rates (0.05, 0.1, 0.5, and 1 MPa/s) on the mechanical properties and acoustic emission (AE) characteristics of modified phosphogypsum were systematically studied through uniaxial compression tests combined with AE technology. The results showed that (1) the peak strength and elastic modulus of MPG increased as a power function of the loading rate, while the peak strain gradually decreased. (2) The cumulative event count of AE decreased as a power function with an increasing loading rate. Compared to the lowest loading rate, the cumulative event count was reduced by nearly two orders of magnitude. (3) An increase in the loading rate resulted in greater large-scale macroscopic failure in MPG specimens, along with an increased proportion of low-frequency AE signals and tensile cracks. (4) The -value of AE decreased with an increasing loading rate, suggesting that microcrack-dominated small-scale damage prevailed at low loading rates, whereas large-scale damage became more pronounced at high loading rates. The abrupt drop in the -value served as a precursor signal for macroscopic failure. This study presents an innovative methodology combining variable loading rates with AE technology to investigate the mechanical response of MPG, and the findings reveal the influence of the loading rate on the mechanical properties and AE characteristics of MPG, providing a theoretical basis for its engineering application under different loading environments.
改性磷石膏(MPG)是一种新型固体废弃物,在复杂应力条件下可呈现出独特的力学性能。本研究通过单轴压缩试验结合声发射(AE)技术,系统研究了不同加载速率(0.05、0.1、0.5和1MPa/s)对改性磷石膏力学性能和声发射特性的影响。结果表明:(1)MPG的峰值强度和弹性模量随加载速率呈幂函数增加,而峰值应变逐渐减小。(2)AE的累计事件数随加载速率增加呈幂函数减少。与最低加载速率相比,累计事件数减少了近两个数量级。(3)加载速率的增加导致MPG试样出现更大规模的宏观破坏,同时低频AE信号和拉伸裂纹的比例增加。(4)AE的b值随加载速率增加而降低,表明在低加载速率下以微裂纹为主的小规模损伤占主导,而在高加载速率下大规模损伤更为明显。b值的突然下降是宏观破坏的前兆信号。本研究提出了一种将可变加载速率与AE技术相结合的创新方法来研究MPG的力学响应,研究结果揭示了加载速率对MPG力学性能和声发射特性的影响,为其在不同加载环境下的工程应用提供了理论依据。