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后固化时间对不同3D打印及传统临时冠材料的光学和力学性能以及化学结构的影响评估

Evaluation of the Effect of Post-Curing Times on the Optical and Mechanical Properties and the Chemical Structure of Different 3D-Printed and Conventional Temporary Crown Materials.

作者信息

Tosun Büşra, Uysal Nur, Özdoğan Alper, Kayır Ömer

出版信息

Int J Prosthodont. 2025 Jun 20;0(0):1-31. doi: 10.11607/ijp.9377.

Abstract

PURPOSE

This study evaluated the effect of post-printing treatment conditions, including curing time, on the optical and mechanical properties of temporary crown (TC) materials.

MATERIALS AND METHODS

A total of 108 specimens of TC materials (PowerResins Temp, PioNext Temporary Restoration Resin, and conventional polymethyl methacrylate (PMMA) were produced. The 3D-printed specimens were post-cured for different time durations (0, 15, 30, and 45 min) (n = 11). During the evaluation of optical properties, color measurement and translucency measurement were performed, while surface hardness and flexural strength were tested mechanically. For structural characterization, analyses were carried out using Fourier Transform Infrared Spectroscopy (FTIR) and scanning electron microscopy. Data was analyzed with an analysis of variance (ANOVA) (P = .05).

RESULTS

The highest color change was observed in the PioNext Temporary Restoration Resin cured for 15 minutes (11.81 ± 0.95), while the lowest was in the non-cured PowerResins Temp group (1.93 ± 0.38) (P < .001). Hardness and flexural strength increased significantly with curing duration (P < .001). FTIR analysis revealed optimal polymerization at 30 min, suggesting this duration offers a clinically favorable balance of mechanical, optical, and chemical properties.

CONCLUSIONS

Both post-curing times and different production techniques affected the microstructural, optical, and mechanical properties of the tested samples. Although longer curing time improved the mechanical properties of the materials, chemical analysis showed that 45 min of curing negatively affected the polymerization. Moreover, curing for 30 min had a positive effect on the mechanical properties without changing the chemical structure of the samples.

摘要

目的

本研究评估了后打印处理条件(包括固化时间)对临时冠(TC)材料光学和机械性能的影响。

材料与方法

共制作了108个TC材料样本(PowerResins Temp、PioNext临时修复树脂和传统聚甲基丙烯酸甲酯(PMMA))。3D打印的样本进行不同时长(0、15、30和45分钟)的后固化处理(n = 11)。在评估光学性能时,进行了颜色测量和透明度测量,同时对表面硬度和弯曲强度进行了机械测试。为进行结构表征,使用傅里叶变换红外光谱(FTIR)和扫描电子显微镜进行分析。数据采用方差分析(ANOVA)进行分析(P = 0.05)。

结果

在固化15分钟的PioNext临时修复树脂中观察到最高的颜色变化(11.81 ± 0.95),而在未固化的PowerResins Temp组中最低(1.93 ± 0.38)(P < 0.001)。硬度和弯曲强度随固化时长显著增加(P < 0.001)。FTIR分析显示在30分钟时聚合效果最佳,表明该时长在机械、光学和化学性能方面提供了临床上有利的平衡。

结论

后固化时间和不同的生产技术均影响了测试样本的微观结构、光学和机械性能。虽然较长的固化时间改善了材料的机械性能,但化学分析表明45分钟的固化对聚合产生了负面影响。此外,30分钟的固化对机械性能有积极影响,且未改变样本的化学结构。

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