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成型角度、打印层厚度和老化对用于临时修复体的打印树脂的弯曲强度、精度、粗糙度和孔隙率分析的影响。

Influence of build angle, printing layer thickness and aging on the flexural strength, precision, roughness and porosity analysis of a printed resin for provisional restorations.

作者信息

de Gois Moreira Fernanda Gurgel, Bezerra Marcella Guedes Pereira Gouvêa, de Miranda Larissa Mendonça, da Silva Sarah Emille Gomes, de Andrade Dantas Eugênia Livia, de Sousa Frederico Barbosa, Özcan Mutlu, E Souza Rodrigo Othávio de Assunção

机构信息

Department of Dentistry, Federal University of Rio Grande Do Norte (UFRN), Av. Salgado Filho Lagoa Nova, Natal, Rio Grande do Norte, 1787CEP: 59056-000, Brazil.

Department of Restorative Dentistry, Federal University of Paraiba (UFPB), João Pessoa, Brazil.

出版信息

Odontology. 2025 Jul;113(3):1165-1179. doi: 10.1007/s10266-025-01060-1. Epub 2025 Feb 1.

Abstract

Evaluate the impact of printing parameters on flexural strength (σ), flexural modulus (E), precision, and surface topography characteristics of a resin used to produce provisional restorations. 450 bars for provisional restorations were printed using the SLA printing (25 × 2x2mm ISO-4049), and randomly divided into 30 groups (n = 15) according to the following factors: "printing layer thickness" (25 μm;50 μm;100 μm), "Build angle" (0°,30°,45°,60°,90°) and "thermocycling-TC" (with or without). Following printing, the samples underwent cleaning with isopropyl alcohol. Photopolymerization was performed for 15 min with an UV lamp. Subsequently, each bar was assessed using a digital caliper at 11 specific points in three dimensions for comparison with the STL file area for precision analysis. Half of the samples underwent thermocycling. All samples were submitted to the σ test. Data for σ (MPa), and (GPa) and precision (mm) were analyzed using 3 and 2-way ANOVA, respectively, and Tukey's post hoc test (5%). Micro-CT, 3D profilometry, and SEM were also performed and analyzed descriptively. The 90°/25μm (63.0 ± 4.5) showed the highest σ, being only statistically similar to the 45°/25μm (57.7 ± 3.1). For precision 0°/25 μm (-2.56 ± 0.04) expressed the greatest variation to the other experimental groups with a sample shrinkage of 25.6% compared to the STL file. The profilometry revealed that the 30º/25 μm group showed prominent peaks and valleys, presenting elevated roughness values with an average of Sa (28.25 μm). Moreover, it was observed that the groups with a 60° angle presented the lowest porosity values. A print layer thickness of 25 μm combined with a build angle of 90º and 45º resulted in higher σ and greater precision.

摘要

评估打印参数对用于制作临时修复体的树脂的弯曲强度(σ)、弯曲模量(E)、精度和表面形貌特征的影响。使用SLA打印(25×2×2mm ISO-4049)制作450个临时修复体的试条,并根据以下因素随机分为30组(n = 15):“打印层厚度”(25μm;50μm;100μm)、“构建角度”(0°、30°、45°、60°、90°)和“热循环-TC”(有或无)。打印后,样品用异丙醇清洗。用紫外线灯进行光聚合15分钟。随后,使用数字卡尺在三个维度的11个特定点对每个试条进行评估,以与STL文件区域进行比较以进行精度分析。一半的样品进行热循环。所有样品均进行σ测试。分别使用三因素和两因素方差分析以及Tukey事后检验(5%)分析σ(MPa)、E(GPa)和精度(mm)的数据。还进行了微型CT、三维轮廓仪和扫描电子显微镜分析,并进行了描述性分析。90°/25μm(63.0±4.5)显示出最高的σ,仅在统计学上与45°/25μm(57.7±3.1)相似。对于精度,0°/25μm(-2.56±0.04)与其他实验组相比变化最大,与STL文件相比样品收缩率为25.6%。轮廓仪显示,30º/25μm组显示出明显的峰谷,粗糙度值升高,平均Sa为(28.25μm)。此外,观察到60°角的组孔隙率值最低。25μm的打印层厚度与90º和45º的构建角度相结合可产生更高的σ和更高的精度。

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