Idris Alisha Ono, Rodrigues Shobha J, Hegde Puneeth, Shetty Thilak, Pai Umesh Y, Saldanha Sharon, M Mahesh, Mukherjee Sandipan, Sales Ann, Kamath Vignesh, Bajantri Prashant
Department of Prosthodontics, Manipal College of Dental Sciences Mangalore, Manipal Academy of Higher Education, Manipal 576104, Karnataka, India.
Int J Dent. 2025 Jun 16;2025:3644666. doi: 10.1155/ijod/3644666. eCollection 2025.
To evaluate the effect of various surface treatments and saliva contamination on the shear bond strength (SBS) and surface characteristics of yttria-stabilized tetragonal zirconia ceramics (YTZP) bonded with self-adhesive resin cement (SAC). Opaque Y-ZTP ceramics were divided into four groups based on specific surface treatment: control (C), air abrasion (AA), G-multiprimer (G), and AA + G (AG). Surface characteristics of the treated specimens, roughness and, elemental analysis were done using scanning electron microscopy (SEM), atomic force microscopy (AFM), and energy dispersive analysis of X-rays (EDAX), respectively. These specimens were further divided into saliva (S) and non-S (NS) contamination groups. Following the surface treatment, 10 resin cement cylinders were affixed onto the zirconia discs within every group. Micro-SBS (µSBS) was calculated, and fracture surfaces were assessed. Statistical analysis was done using one-way analysis of variance (ANOVA) and the post hoc Tukey test. The µSBS values for the groups were as follows: CS (0.86 ± 0.7), CNS (3.13 ± 2.7), AS (3.14 ± 2.6), ANS (2.96 ± 1.2), GS (5.92 ± 2.2), GNS (5.94 ± 2.2), AGS (4.97 ± 0.9), and AGNS (8.06 ± 1.4). A one-way ANOVA showed that all the groups had a statistically significant difference in the SBS except the AS, AGS, CNS, ANS, as well as the GNS and AGNS. AFM results revealed the mean roughness value of AA is highest, followed by G-multiprimer, AG, and least in control. This difference is statistically significant with -value of <0.001. This also correlated with the SEM images. Airborne particle abrasion and the application of G-multiprimer provide the best results in a moisture-free environment.
评估各种表面处理和唾液污染对氧化钇稳定四方氧化锆陶瓷(YTZP)与自粘树脂水门汀(SAC)粘结的剪切粘结强度(SBS)和表面特性的影响。根据特定表面处理将不透明的Y-ZTP陶瓷分为四组:对照组(C)、空气喷砂(AA)、G-多重底漆(G)和AA + G(AG)。分别使用扫描电子显微镜(SEM)、原子力显微镜(AFM)和X射线能谱分析(EDAX)对处理后的试样进行表面特性、粗糙度和元素分析。这些试样进一步分为唾液污染(S)组和非唾液污染(NS)组。表面处理后,在每组的氧化锆盘上粘贴10个树脂水门汀圆柱体。计算微剪切粘结强度(µSBS),并评估断裂表面。使用单因素方差分析(ANOVA)和事后Tukey检验进行统计分析。各组的µSBS值如下:CS(0.86±0.7)、CNS(3.13±2.7)、AS(3.14±2.