Xing Chengwei, Chang Zhibin, Zhu Bohan, Jin Tian, Ma Qing, Wang Jie
Key Laboratory for Special Area Highway Engineering, Ministry of Education, Chang'an University, South 2nd Ring Road Middle Section, Xi'an 710064, China.
School of Highway, Chang'an University, South 2nd Ring Road Middle Section, Xi'an 710064, China.
Materials (Basel). 2025 Jun 13;18(12):2785. doi: 10.3390/ma18122785.
This paper aims to explore the influences of the content and gradation of mineral powder on the rheological properties of styrene-butadiene-styrene (SBS) modified asphalt mastic at different aging stages and temperatures. In the experiment, SBS modified asphalt mastic samples with different powder-to-binder ratios (0.6, 0.8, and 1.0) and different mineral powder gradations (500 mesh passing rates of 76.89% and 100%) were prepared. Following aging periods of 5, 25, and 45 h in the pressure aging vessel (PAV), the asphalt underwent comprehensive rheological characterization using a dynamic shear rheometer (DSR). The research shows that mineral powder can boost mastic's deformation resistance and elastic effect. When aged by PAV for 45 h, the powder-to-binder ratio increased from 0.6 to 1.0, and its complex modulus increased by nearly 2.5 times at 58 °C. For SBS modified asphalt mastic of PAV 0 h, the powder-to-binder ratio increased from 0.6 to 1.0 and its phase angle was reduced from 59.6 to 53.2, which indicated that the elasticity of mastic was improved. However, this accelerated the degradation rate of SBS, making the aging process more complex. Fine-grained mineral powder is more effective in enhancing mastic's deformation resistance than coarse-grained mineral powder. The fine-graded mastic had better rutting resistance after 45 h of aging than after 25 h of aging because the mineral powder compensated for the SBS loss-induced elasticity reduction. Smaller mineral powder particles lead to better a mastic anti-aging effect. After 45 h of aging, fine-grained mineral powder offered a better elastic effect. But the ways in which mineral powder and SBS boost mastic elasticity differ greatly. The results of this study provide a reference for optimizing the design of asphalt mixtures.
本文旨在探究矿粉含量和级配在不同老化阶段及温度下对苯乙烯-丁二烯-苯乙烯(SBS)改性沥青玛蹄脂流变性能的影响。实验中制备了不同粉胶比(0.6、0.8和1.0)以及不同矿粉级配(500目通过率分别为76.89%和100%)的SBS改性沥青玛蹄脂样品。在压力老化容器(PAV)中老化5、25和45小时后,使用动态剪切流变仪(DSR)对沥青进行全面的流变特性表征。研究表明,矿粉可提高玛蹄脂的抗变形能力和弹性效果。经PAV老化45小时后,粉胶比从0.6增加到1.0,在58℃时其复数模量增加了近2.5倍。对于PAV老化0小时的SBS改性沥青玛蹄脂,粉胶比从0.6增加到1.0,其相位角从59.6降至53.2,这表明玛蹄脂的弹性得到了改善。然而,这加速了SBS的降解速率,使老化过程更加复杂。细颗粒矿粉在增强玛蹄脂抗变形能力方面比粗颗粒矿粉更有效。细级配玛蹄脂在老化45小时后的抗车辙性能比老化25小时后更好,因为矿粉弥补了因SBS损失导致的弹性降低。较小的矿粉颗粒导致更好的玛蹄脂抗老化效果。老化45小时后,细颗粒矿粉具有更好的弹性效果。但矿粉和SBS提高玛蹄脂弹性的方式有很大差异。本研究结果为优化沥青混合料设计提供了参考。