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新型生物活性修复材料的离子释放、显微硬度及抗釉质脱矿性能

Ion Release, Microhardness and Enamel Demineralization Resistance of New Bioactive Restorative Materials.

作者信息

Maaly Tayseer, Darweesh Fawzy A, Elnawawy Mohamed Samir

机构信息

Dental Biomaterials, Faculty of Dentistry, Zagazig University, Egypt.

Oral Biology Department, Faculty of Dentistry, Zagazig University, Egypt.

出版信息

J Clin Exp Dent. 2025 Jun 1;17(6):e656-e664. doi: 10.4317/jced.62357. eCollection 2025 Jun.

Abstract

BACKGROUND

The objective of the study was to assess fluoride and calcium release from new bioactive materials and to correlate the results with surface hardness and enamel demineralization resistance.

MATERIAL AND METHODS

Three ion releasing restorative materials were considered: Surefil one (SO), Equia forte fil HT (EF), and Activa bioactive resorative (AB). Baseline microhardness (MH) of the restorative materials was recorded. The amount of released fluoride and calcium ions and microhardness of the materials were estimated at different intervals of 7,14 and 21 days storage in distallid water. Ion release values were recorded using Ionchromatography. Finally, enamel demineralization resistance was evaluated using a microhardness tester. Enamel surface morphology, calcium and phosphorous wt. % were evaluated utilizing the scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM\EDX).

RESULTS

SO released more fluoride and lower calcium ions than the other groups (< 0.05). EF recorded more fluoride and calcium ion release compared to AB. The highest MH values at all intervals were for SO followed by EF, both materials exhibited significant MH increase upon storage. AB exhibited the lowest MH which decreased upon storage. In the acid resistance test, EF showed effective resistance to demineralization followed by AB.

CONCLUSIONS

EF is an effective restorative material when applied in cariogenic media with adequate surface hardness qualities upon storage. Bioactive material, Ion release, Enamel demineralization resistance, Microhardness.

摘要

背景

本研究的目的是评估新型生物活性材料中氟和钙的释放情况,并将结果与表面硬度和牙釉质抗脱矿能力相关联。

材料与方法

研究了三种离子释放型修复材料:Surefil one(SO)、Equia forte fil HT(EF)和Activa生物活性修复材料(AB)。记录了修复材料的基线显微硬度(MH)。在蒸馏水中储存7、14和21天的不同时间间隔,估计材料中氟离子和钙离子的释放量以及材料的显微硬度。使用离子色谱法记录离子释放值。最后,使用显微硬度测试仪评估牙釉质抗脱矿能力。利用扫描电子显微镜和能量色散X射线光谱仪(SEM\EDX)评估牙釉质表面形态、钙和磷的重量百分比。

结果

与其他组相比,SO释放的氟更多,钙离子更少(<0.05)。与AB相比,EF记录的氟离子和钙离子释放更多。所有时间间隔内,SO的MH值最高,其次是EF,两种材料在储存后MH均显著增加。AB的MH最低,且在储存后降低。在耐酸性测试中,EF表现出有效的抗脱矿能力,其次是AB。

结论

EF是一种有效的修复材料,当应用于致龋介质中时,储存后具有足够的表面硬度质量。生物活性材料、离子释放、牙釉质抗脱矿能力、显微硬度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3fb5/12225766/1d46d3238835/jced-17-06-e656-g001.jpg

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