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传统聚甲基丙烯酸甲酯与微晶纤维素增强聚甲基丙烯酸甲酯表面粗糙度和冲击强度的比较评估——一项体外研究。

Comparative evaluation of surface roughness and impact strength of conventional polymethyl methacrylate and microcrystalline cellulose reinforced polymethyl methacrylate - An in vitro study.

作者信息

Reddy Thumma Sagar, George Vinu Thomas, Shahi Gauri, Ray Sauptik

机构信息

Department of Prosthodontics and Crown and Bridge, Manipal College of Dental Sciences, Manipal, Manipal Academy of Higher Education, Manipal, Karnataka, India.

Department of Dental and Prosthetic Surgery, Homi Bhabha Cancer Hospital and Research Centre, Tata Memorial Centre, Visakhapatnam, Andhra Pradesh, India.

出版信息

J Indian Prosthodont Soc. 2025 Jul 1;25(3):204-209. doi: 10.4103/jips.jips_459_24. Epub 2025 Jul 16.

Abstract

AIM

To evaluate and compare the surface roughness and impact strength of conventional polymethyl methacrylate (PMMA) with microcrystalline cellulose (MCC)-reinforced PMMA.

SETTINGS AND DESIGN

An in-vitro experimental study was conducted. Fifty PMMA specimens were fabricated and divided into five groups based on MCC concentration (2% or 5%) and particle size (20 μm or 50 μm).

MATERIALS AND METHODS

Specimens (80 mm × 10 mm × 4 mm) were categorized as follows: Group A (control; conventional PMMA), Groups B and D (2% MCC with 20 µm and 50 µm particles, respectively), and Groups C and E (5% MCC with 20 µm and 50 µm particles, respectively). Surface roughness was measured using a contact profilometer, and impact strength was tested with a ZwickRoell impact testing machine.

STATISTICAL ANALYSIS USED

Statistical analysis was performed using IBM SPSS Version 28.0. One-way ANOVA followed by Tukey's post hoc test was used to determine intergroup differences, with the significance level set at p<0.05.

RESULTS

Surface roughness was lower in Groups B (0.89±0.43), C (1.07±0.34), and E (0.77±0.27) compared to the control Group A (1.25±0.42), while Group D (1.84±0.25) showed higher values. Impact strength in Groups C (1.85±0.23), D (1.80±0.17), and E (1.81±0.26) was slightly lower than the control (1.88±0.31), though not statistically significant. However, Group B (1.56 ± 0.20) showed a significant reduction.

CONCLUSION

The addition of 20 μm MCC reduced surface roughness at both 2% and 5% concentrations, whereas 50 μm MCC increased roughness at 2% but decreased at 5%. Impact strength remained comparable to the control in all groups except PMMA + 2% MCC (20 μm), which exhibited a significant decline. MCC reinforcement influences PMMA's mechanical and surface properties, suggesting its potential for denture base modifications.

摘要

目的

评估并比较传统聚甲基丙烯酸甲酯(PMMA)与微晶纤维素(MCC)增强PMMA的表面粗糙度和冲击强度。

设置与设计

进行一项体外实验研究。制作了50个PMMA标本,并根据MCC浓度(2%或5%)和粒径(20μm或50μm)分为五组。

材料与方法

标本(80mm×10mm×4mm)分类如下:A组(对照组;传统PMMA),B组和D组(分别为含20μm和50μm颗粒的2% MCC),以及C组和E组(分别为含20μm和50μm颗粒的5% MCC)。使用接触式轮廓仪测量表面粗糙度,并用ZwickRoell冲击试验机测试冲击强度。

所用统计分析方法

使用IBM SPSS 28.0版进行统计分析。采用单因素方差分析,随后进行Tukey事后检验以确定组间差异,显著性水平设定为p<0.05。

结果

与对照组A组(1.25±0.42)相比,B组(0.89±0.43)、C组(1.07±0.34)和E组(0.77±0.27)的表面粗糙度较低,而D组(1.84±0.25)的值较高。C组(1.85±0.23)、D组(1.80±0.17)和E组(1.81±0.26)的冲击强度略低于对照组(1.88±0.31),但无统计学意义。然而,B组(1.56±0.20)显示出显著降低。

结论

添加20μm的MCC在2%和5%浓度下均降低了表面粗糙度,而50μm的MCC在2%时增加了粗糙度,但在5%时降低了粗糙度。除PMMA + 2% MCC(20μm)组显著下降外,所有组的冲击强度与对照组相当。MCC增强影响了PMMA的机械性能和表面性能,表明其在义齿基托改性方面的潜力。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2420/12370108/efb32d1b80a9/JIPS-25-204-g001.jpg

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