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氧化镎纳米颗粒的合成工程

Synthetic engineering of neptunium oxide nanoparticles.

作者信息

Hastings Ashley M, Cicchetti Nic, Boro Joseph R, Parsons-Davis Tashi, Shusterman Jennifer A

机构信息

Nuclear and Chemical Sciences Division, Lawrence Livermore National Laboratory Livermore CA 94550 USA

University of Nevada Las Vegas Las Vegas NV 89154 USA.

出版信息

Nanoscale Adv. 2025 Jul 16;7(16):4848-4851. doi: 10.1039/d5na00523j. eCollection 2025 Aug 5.

DOI:10.1039/d5na00523j
PMID:40677900
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12266061/
Abstract

Spherical neptunium oxide nanoparticles in the 40-200 nm size range are synthesized through a homogeneous precipitation approach. These particles and their suspensions are characterized with various spectroscopic and microscopic analyses. This work bridges a gap in available size regimes for structure-property relationships in nuclear materials.

摘要

通过均匀沉淀法合成了尺寸范围在40 - 200纳米的球形氧化镎纳米颗粒。这些颗粒及其悬浮液通过各种光谱和显微镜分析进行了表征。这项工作填补了核材料结构 - 性能关系中现有尺寸范围的空白。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/76af56d08c48/d5na00523j-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/343aeab20d33/d5na00523j-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/6807248a5a7c/d5na00523j-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/01e93d2bd260/d5na00523j-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/76af56d08c48/d5na00523j-f4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/343aeab20d33/d5na00523j-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/6807248a5a7c/d5na00523j-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/01e93d2bd260/d5na00523j-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9b42/12323834/76af56d08c48/d5na00523j-f4.jpg

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本文引用的文献

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Quantitative Particle Analysis of Neptunium-237 Oxides: Optimization of MAMA Analysis for Modified Direct Denitration Products.
Microsc Microanal. 2025 Feb 17;31(1). doi: 10.1093/mam/ozae112.
2
Formation of Fully Stoichiometric, Oxidation-State Pure Neptunium and Plutonium Dioxides from Molecular Precursors.由分子前驱体形成化学计量比完全、氧化态纯净的镎和钚的二氧化物。
Inorg Chem. 2024 Sep 30;63(39):18417-18428. doi: 10.1021/acs.inorgchem.4c02099. Epub 2024 Sep 16.
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Preparation of monodisperse cerium oxide particle suspensions from a tetravalent precursor.
Dalton Trans. 2024 Apr 30;53(17):7376-7383. doi: 10.1039/d4dt00146j.
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Transforming lanthanide and actinide chemistry with nanoparticles.用纳米颗粒改变镧系元素和锕系元素化学。
Nanoscale. 2020 Jan 23;12(3):1339-1348. doi: 10.1039/c9nr09175k.
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Intrinsic formation of nanocrystalline neptunium dioxide under neutral aqueous conditions relevant to deep geological repositories.
Chem Commun (Camb). 2015 Jan 25;51(7):1301-4. doi: 10.1039/c4cc08103j.
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Plutonium transport in the environment.钚在环境中的迁移。
Inorg Chem. 2013 Apr 1;52(7):3533-46. doi: 10.1021/ic3018908. Epub 2013 Mar 4.
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Gold coated lanthanide phosphate nanoparticles for targeted alpha generator radiotherapy.金包覆的镧系磷酸盐纳米颗粒用于靶向α放射源治疗。
PLoS One. 2013;8(1):e54531. doi: 10.1371/journal.pone.0054531. Epub 2013 Jan 18.
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Microsc Microanal. 2010 Feb;16(1):13-20. doi: 10.1017/S1431927609991206. Epub 2009 Dec 24.
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Particle size distribution measurements of manganese-doped ZnS nanoparticles.锰掺杂硫化锌纳米颗粒的粒度分布测量
Anal Chem. 2009 May 15;81(10):3889-95. doi: 10.1021/ac900043y.