• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

一种通过掠入射X射线衍射对薄膜进行定量取向和相分数分析的系统方法。

A systematic approach for quantitative orientation and phase fraction analysis of thin films through grazing-incidence X-ray diffraction.

作者信息

Gasser Fabian, John Sanjay, Smets Jorid, Simbrunner Josef, Fratschko Mario, Rubio-Giménez Víctor, Ameloot Rob, Steinrück Hans-Georg, Resel Roland

机构信息

Institute of Solid State Physics Graz University of Technology Petersgasse 16 8010Graz Austria.

Center for Membrane Separations, Adsorption, Catalysis and Spectroscopy (cMACS) KU Leuven Celestijnenlaan 200f 3001Leuven Belgium.

出版信息

J Appl Crystallogr. 2025 Jul 22;58(Pt 4):1288-1298. doi: 10.1107/S1600576725004935. eCollection 2025 Aug 1.

DOI:10.1107/S1600576725004935
PMID:40765963
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12321010/
Abstract

Grazing-incidence X-ray diffraction (GIXD) is widely used for the structural characterization of thin films, particularly for analyzing phase composition and the orientation distribution of crystallites. While various tools exist for qualitative evaluation, a widely applicable systematic procedure to obtain quantitative information has not yet been developed. This work presents a first step in that direction, allowing accurate quantitative information to be obtained through the evaluation of radial line profiles from GIXD data. An algorithm is introduced for computing radial line profiles based on the crystal structure of known compounds. By fitting experimental data with calculated line profiles, accurate quantitative information about orientation distribution and phase composition is obtained, along with additional parameters such as mosaicity and total crystal volume. The approach is demonstrated using three distinct thin film systems, highlighting the broad applicability of the algorithm. This method provides a systematic and general approach to obtaining quantitative information from GIXD data.

摘要

掠入射X射线衍射（GIXD）被广泛用于薄膜的结构表征，特别是用于分析相组成和微晶的取向分布。虽然存在各种用于定性评估的工具，但尚未开发出一种广泛适用的获取定量信息的系统程序。这项工作朝着这个方向迈出了第一步，通过评估GIXD数据的径向线轮廓来获得准确的定量信息。引入了一种基于已知化合物晶体结构计算径向线轮廓的算法。通过将实验数据与计算出的线轮廓进行拟合，可以获得关于取向分布和相组成的准确定量信息，以及诸如镶嵌性和总晶体体积等附加参数。使用三个不同的薄膜系统对该方法进行了演示，突出了该算法的广泛适用性。该方法提供了一种从GIXD数据中获取定量信息的系统通用方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/e4e0e5a020b8/j-58-01288-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/4fd83fff87d3/j-58-01288-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/b9237ad1839d/j-58-01288-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/edab6a2c8b72/j-58-01288-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/d09c1f153207/j-58-01288-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/3e84e21501e3/j-58-01288-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/e4e0e5a020b8/j-58-01288-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/4fd83fff87d3/j-58-01288-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/b9237ad1839d/j-58-01288-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/edab6a2c8b72/j-58-01288-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/d09c1f153207/j-58-01288-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/3e84e21501e3/j-58-01288-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/9d0b/12321010/e4e0e5a020b8/j-58-01288-fig6.jpg

相似文献

1
A systematic approach for quantitative orientation and phase fraction analysis of thin films through grazing-incidence X-ray diffraction.一种通过掠入射X射线衍射对薄膜进行定量取向和相分数分析的系统方法。
J Appl Crystallogr. 2025 Jul 22;58(Pt 4):1288-1298. doi: 10.1107/S1600576725004935. eCollection 2025 Aug 1.
2
Short-Term Memory Impairment短期记忆障碍
3
[Volume and health outcomes: evidence from systematic reviews and from evaluation of Italian hospital data].[容量与健康结果：来自系统评价和意大利医院数据评估的证据]
Epidemiol Prev. 2013 Mar-Jun;37(2-3 Suppl 2):1-100.
4
Management of urinary stones by experts in stone disease (ESD 2025).结石病专家对尿路结石的管理（2025年结石病专家共识）
Arch Ital Urol Androl. 2025 Jun 30;97(2):14085. doi: 10.4081/aiua.2025.14085.
5
A rapid and systematic review of the clinical effectiveness and cost-effectiveness of paclitaxel, docetaxel, gemcitabine and vinorelbine in non-small-cell lung cancer.对紫杉醇、多西他赛、吉西他滨和长春瑞滨在非小细胞肺癌中的临床疗效和成本效益进行的快速系统评价。
Health Technol Assess. 2001;5(32):1-195. doi: 10.3310/hta5320.
6
Sexual Harassment and Prevention Training性骚扰与预防培训
7
Health professionals' experience of teamwork education in acute hospital settings: a systematic review of qualitative literature.医疗专业人员在急症医院环境中团队合作教育的经验：对定性文献的系统综述
JBI Database System Rev Implement Rep. 2016 Apr;14(4):96-137. doi: 10.11124/JBISRIR-2016-1843.
8
Eliciting adverse effects data from participants in clinical trials.从临床试验参与者中获取不良反应数据。
Cochrane Database Syst Rev. 2018 Jan 16;1(1):MR000039. doi: 10.1002/14651858.MR000039.pub2.
9
Cost-effectiveness of using prognostic information to select women with breast cancer for adjuvant systemic therapy.利用预后信息为乳腺癌患者选择辅助性全身治疗的成本效益
Health Technol Assess. 2006 Sep;10(34):iii-iv, ix-xi, 1-204. doi: 10.3310/hta10340.
10
The Lived Experience of Autistic Adults in Employment: A Systematic Search and Synthesis.成年自闭症患者的就业生活经历：系统检索与综述
Autism Adulthood. 2024 Dec 2;6(4):495-509. doi: 10.1089/aut.2022.0114. eCollection 2024 Dec.

本文引用的文献

1
Intensity corrections for grazing-incidence X-ray diffraction of thin films using static area detectors.使用静态面积探测器对薄膜掠入射X射线衍射进行强度校正。
J Appl Crystallogr. 2025 Feb 1;58(Pt 1):96-106. doi: 10.1107/S1600576724010628.
2
Thin Film Formation Based on a Nanoporous Metal-Organic Framework by Layer-By-Layer Deposition.基于纳米多孔金属有机框架通过逐层沉积形成薄膜。
ACS Appl Nano Mater. 2024 Nov 1;7(22):25645-25654. doi: 10.1021/acsanm.4c04763. eCollection 2024 Nov 22.
3
Evolution of Defects, Morphology, and Strain during FAMAPbI Perovskite Vacuum Deposition: Insights from In Situ Photoluminescence and X-ray Scattering.
FAMAPbI钙钛矿真空沉积过程中缺陷、形态和应变的演变：原位光致发光和X射线散射的见解
ACS Appl Mater Interfaces. 2024 Jul 10;16(27):35723-35731. doi: 10.1021/acsami.4c04095. Epub 2024 Jun 27.
4
: heuristic tool for the efficient reduction of grazing-incidence X-ray scattering data.用于高效简化掠入射X射线散射数据的启发式工具。
J Appl Crystallogr. 2024 Feb 12;57(Pt 2):509-528. doi: 10.1107/S1600576723011159. eCollection 2024 Apr 1.
5
A Systematic Review of Metal Halide Perovskite Crystallization and Film Formation Mechanism Unveiled by In Situ GIWAXS.原位掠入射广角X射线散射揭示金属卤化物钙钛矿结晶和薄膜形成机制的系统综述
Adv Mater. 2021 Dec;33(51):e2105290. doi: 10.1002/adma.202105290. Epub 2021 Oct 4.
6
MXene-Copper/Cobalt Hybrids via Lewis Acidic Molten Salts Etching for High Performance Symmetric Supercapacitors.通过路易斯酸性熔盐蚀刻制备用于高性能对称超级电容器的MXene-铜/钴杂化物
Angew Chem Int Ed Engl. 2021 Nov 22;60(48):25318-25322. doi: 10.1002/anie.202112381. Epub 2021 Oct 21.
7
Oriented Growth of In-Oxo Chain Based Metal-Porphyrin Framework Thin Film for High-Sensitive Photodetector.用于高灵敏度光电探测器的基于In-Oxo链的金属卟啉框架薄膜的定向生长
Adv Sci (Weinh). 2021 May 17;8(14):2100548. doi: 10.1002/advs.202100548. eCollection 2021 Jul.
8
Time-Resolved Structural Kinetics of an Organic Mixed Ionic-Electronic Conductor.有机混合离子-电子导体的时间分辨结构动力学
Adv Mater. 2020 Oct;32(40):e2003404. doi: 10.1002/adma.202003404. Epub 2020 Aug 30.
9
: a comprehensive software tool for geometry-independent grazing-incidence X-ray diffraction data analysis and pole-figure calculations.一款用于与几何无关的掠入射X射线衍射数据分析和极图计算的综合软件工具。
J Appl Crystallogr. 2019 May 31;52(Pt 3):683-689. doi: 10.1107/S1600576719004485. eCollection 2019 Jun 1.
10
Kinetics of Ion-Exchange Reactions in Hybrid Organic-Inorganic Perovskite Thin Films Studied by In Situ Real-Time X-ray Scattering.通过原位实时X射线散射研究杂化有机-无机钙钛矿薄膜中离子交换反应的动力学
J Phys Chem Lett. 2018 Dec 6;9(23):6750-6754. doi: 10.1021/acs.jpclett.8b02916. Epub 2018 Nov 13.