Al-Haddad Juman, Najmafshar Nafiseh, Ritter Andre V, Sadr Alireza
Biomimetics Biomaterials Biophotonics Biomechanics & Technology (B4T), Department of Restorative Dentistry, University of Washington, 1959 NE Pacific St., Seattle, WA 98195, USA.
Materials (Basel). 2025 Aug 12;18(16):3790. doi: 10.3390/ma18163790.
Polymerization shrinkage in resin-based composites can lead to gap formation at the tooth-restoration interface, potentially compromising the long-term success of restorations. Bulk-fill composites have been developed to reduce shrinkage stress, but their adaptation and bond strength-especially in deep cavities-remain areas of concern. This study investigated the adaptation and bond strength of a newly developed dual-cure bulk-fill composite in 4 mm deep preparations compared to light-cured and self-adhesive bulk-fill composites in six groups. Standard composite molds were used to observe and measure sealed floor area (SFA%) of the composite after the polymerization process under optical coherence tomography (OCT) imaging. Micro-tensile bond strength (MTBS) testing was conducted in extracted human teeth. OCT showed that the prototype dual-cure composites had the lowest gap formation during polymerization (SFA 91%), while the self-adhesive composite demonstrated the highest debonding from the cavity floor (SFA 26%, < 0.001). For MTBS analysis, the lowest mean bond strength was recorded for the self-adhesive composite (21 MPa) and the highest for a light-cured bulk-fill (50 MPa, < 0.05). Overall, the dual-cure bulk-fill composites exhibited less gap formation than the light-cured ones. The prototype dual-cure material with 90 s waiting before light-curing showed the best adaptation. However, these differences were not reflected in the bond strength values to the cavity floor dentin using the universal adhesive used in the current study, as the light-cured composite showed the highest bond strength values. The self-adhesive composite showed the poorest results in both experiments, indicating that the application of a bonding system is still necessary for better adaptation and bonding to the cavity floor dentin.
树脂基复合材料中的聚合收缩会导致牙齿修复界面出现间隙,这可能会影响修复体的长期成功率。为了降低收缩应力,人们开发了大块充填复合材料,但其适应性和粘结强度,尤其是在深龋洞中的表现,仍然是令人担忧的问题。本研究将一种新开发的双固化大块充填复合材料与光固化和自粘结大块充填复合材料分为六组,研究了其在4mm深的窝洞中制备时的适应性和粘结强度。使用标准复合模具,在光学相干断层扫描(OCT)成像下观察和测量聚合过程后复合材料的封闭底面积(SFA%)。在拔除的人牙上进行微拉伸粘结强度(MTBS)测试。OCT显示,原型双固化复合材料在聚合过程中形成的间隙最小(SFA为91%),而自粘结复合材料从洞底脱粘的情况最为严重(SFA为26%,P<0.001)。对于MTBS分析,自粘结复合材料的平均粘结强度最低(约21MPa),光固化大块充填复合材料的平均粘结强度最高(约50MPa,P<0.05)。总体而言,双固化大块充填复合材料比光固化复合材料形成的间隙更少。在光固化前等待90秒的原型双固化材料表现出最佳的适应性。然而,在本研究中使用通用粘结剂时,这些差异并未反映在与洞底牙本质的粘结强度值上,因为光固化复合材料的粘结强度值最高。自粘结复合材料在两个实验中的结果最差,这表明为了更好地与洞底牙本质贴合和粘结,仍然需要使用粘结系统。