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多模态阻抗和X射线表征能够同时检测整体和界面结晶。

Multi-modal impedance and X-ray characterization enables simultaneous detection of bulk and interfacial crystallization.

作者信息

Doppelhammer Nikolaus, Spira Daniel, Rais Anjul, Vandenabeele Dries, Wangermez Wauter, McMonagle Charles, Chernyshov Dmitry, Breynaert Eric

机构信息

NMRCoRe-NMR/X-Ray platform for Convergence Research, KU Leuven, Leuven 3001, Belgium.

Centre for Surface Chemistry and Catalysis Characterisation and Application Team (COK-KAT), KU Leuven, Leuven 3001, Belgium.

出版信息

Chem Commun (Camb). 2025 Sep 2. doi: 10.1039/d5cc03808a.

DOI:10.1039/d5cc03808a
PMID:40891346
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC12402976/
Abstract

A multi-modal platform enabling simultaneous impedance spectroscopy and X-ray scattering is presented. When applied to zeolite crystallization, four-electrode impedance measurements reliably track bulk crystallization kinetics in agreement with X-ray diffraction, while two-electrode impedance data reveal artefacts from electrode passivation.

摘要

本文介绍了一种能够同时进行阻抗谱和X射线散射的多模态平台。当应用于沸石结晶过程时，四电极阻抗测量能够可靠地追踪整体结晶动力学，与X射线衍射结果一致，而两电极阻抗数据则揭示了电极钝化产生的假象。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/58830dad15b9/d5cc03808a-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/cdde9d06b5e3/d5cc03808a-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/5d69d2f328da/d5cc03808a-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/58830dad15b9/d5cc03808a-f3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/cdde9d06b5e3/d5cc03808a-f1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/5d69d2f328da/d5cc03808a-f2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1897/12402976/58830dad15b9/d5cc03808a-f3.jpg

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Troubleshooting the influence of trace chemical impurities on nanoparticle growth kinetics electrochemical measurements.解决痕量化学杂质对纳米颗粒生长动力学电化学测量的影响。
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Illuminating the Black Box: A Perspective on Zeolite Crystallization in Inorganic Media.
揭开黑箱之谜：无机介质中沸石结晶的视角
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Structural Aspects Affecting Phase Selection in Inorganic Zeolite Synthesis.影响无机沸石合成中相选择的结构因素
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