Kruschwitz Sabine, Munsch Sarah, Telong Melissa, Schmidt Wolfram, Bintz Thilo, Fladt Matthias, Stelzner Ludwig
Bundesanstalt für Materialforschung und -prüfung, Unter den Eichen 87, Berlin, 12205, Germany.
Technische Universität Berlin, Gustav-Meyer-Allee 25, Berlin, 13355, Germany.
Magn Reson Lett. 2023 Apr 7;3(3):207-219. doi: 10.1016/j.mrl.2023.03.004. eCollection 2023 Aug.
NMR is becoming increasingly popular for the investigation of building materials as it is a non-invasive technology that does not require any sample preparation nor causes damage to the material. Depending on the specific application it can offer insights into properties like porosity and spatial saturation degree as well as pore structure. Moreover it enables the determination of moisture transport properties and the (re-)distribution of internal moisture into different reservoirs or chemical phases upon damage and curing. However, as yet most investigations were carried out using devices originally either designed for geophysical applications or the analysis of rather homogeneous small scale (< 10 mL) samples. This paper describes the capabilities of an NMR tomograph, which has been specifically optimized for the investigation of larger, heterogeneous building material samples (diameters of up to 72 mm, length of up to 700 mm) with a high flexibility due to interchangeable coils allowing for a high SNR and short echo times (50-80 μs).
核磁共振(NMR)在建筑材料研究中越来越受欢迎,因为它是一种非侵入性技术,不需要任何样品制备,也不会对材料造成损坏。根据具体应用,它可以提供有关孔隙率、空间饱和度以及孔隙结构等特性的见解。此外,它还能够测定水分传输特性,以及在材料受损和固化时内部水分在不同储层或化学相中的(再)分布。然而,到目前为止,大多数研究都是使用最初设计用于地球物理应用或分析相当均匀的小规模(<10 mL)样品的设备进行的。本文描述了一种NMR断层扫描仪的功能,该扫描仪经过专门优化,用于研究更大的、异质的建筑材料样品(直径可达72毫米,长度可达700毫米),由于采用了可互换线圈,具有很高的灵活性,能够实现高信噪比和短回波时间(50 - 80微秒)。