The Investigation of Shear Fracture Toughness and Structure of ITZ of Limestone Concrete with Different Aggregate Grain Size.

Due to the shortage of construction aggregates, carbonate rock aggregates-including mainly limestone aggregates-have long been used in structural concrete in many countries worldwide. On the other hand, earlier tests on the shear fracture toughness of concretes with limestone aggregates were very limited and were even abandoned for many years. For the above reasons, in this paper, completely new fracture toughness tests were performed according to the mode II fracture for limestone concretes with different grain size distributions. Two types of aggregate grain were used, i.e., two with maximum grain sizes of 8 mm (M1 series concrete) and 16 mm (M2 series concrete). During the experiments, the critical stress-intensity factor () and critical unit work of failure () were determined. Based on the conducted studies, it was found that higher values of fracture mechanics parameters were noted as the grain sizes of the aggregate used increased. The increases in the analyzed fracture mechanics parameters were noticeably greater in the M2 series concrete compared to the results for the M1 series concrete, specifically by 27% for and 35% for . In addition to macroscopic tests, detailed microstructural analyses of the ITZ area between the coarse aggregate grains and the cement matrix were conducted. Based on the captured images, it was determined that, in the M1 series concrete, the contacts between the aggregate grains and the cement paste exhibit a loose structure with visible microcracks. In contrast, the M2 series concrete showed no visible damages within the ITZ area itself nor at their displacement at a distance of approximately a few μm away from this area. This microstructure of both materials resulted in the M1 series concrete being more prone to rapid and sudden fracture propagation, leading to its brittle behavior during the fracture process. In contrast, the large, well-developed limestone aggregate grains in the M2 series concrete facilitated improved stress transfer beyond the ITZ area into the cement matrix, preserving the continuity of the material structure and consequently leading to quasi-plastic behavior of the concrete during the fracture process. The novelty and utilitarianism of the research undertaken result from the fact that exploring the properties of concretes with limestone aggregates using mode II fracture is an important aspect of evaluating the durability and safety of concrete structures subjected mainly to shear forces.