Fan Yunpeng, Zhao Xiaodong, Yu Linjun, Shi Dengwang, Tian Weichao, Wen Zhigang, Liu Yuhang, Gao Yuan, Lv Yiming, Hu Jun
Hubei Key Laboratory of Petroleum Geochemistry and Environment, Yangtze University, Wuhan 430100, People's Republic of China.
School of Resources and Environment, Yangtze University, Wuhan 430100, People's Republic of China.
ACS Omega. 2025 Aug 30;10(36):41370-41385. doi: 10.1021/acsomega.5c04481. eCollection 2025 Sep 16.
Fluid type and content directly control fluid mobility in tight reservoirs. At present, there are two ways to classify fluid types. One is to classify fluids into movable fluids (MF), capillary-bound fluids (CAF), and clay-bound fluids (CLF). The other is to classify fluids into free fluids and adsorbed fluids. However, the intrinsic relationship between the two fluid classification schemes is still unclear. In order to investigate the pore structure and fluid type characteristics, a series of experiments were performed on the Chang 7 tight sandstone in the Longdong area. The full-scale pore size distribution (PSD) can be obtained by combining low-temperature nitrogen adsorption (LTNA) with nuclear magnetic resonance (NMR). The PSD of Chang 7 tight sandstones primarily ranges from 1 nm to 20 μm. Based on the fractal characteristics, pore system is divided into macropores (mainly >150.8 nm), and micropores (mainly <150.8 nm). MF, CLF, and CAF constitute 11.1-49.7% (avg. 34.6%), 17.3-40.1% (avg. 26.7%), and 32.9-48.8% (avg. 38.7%) of total fluid, respectively. Additionally, macropores are positively correlated with MF and negatively correlated with CAF and CLF, whereas micropores show the opposite trend. By integrating NMR data with theoretical modeling, a clear correspondence between the two fluid classification approaches was established: MF and CAF closely correspond to free fluids, while CLF is strongly associated with adsorbed fluids. Notably, in samples with low porosity and extremely fine pore throats, the combination of centrifugation and theoretical modeling may underestimate the actual free fluid content. MF shows a weak negative correlation with quartz and clay minerals; CAF and CLF are weakly positively correlated with quartz and clay but negatively correlated with feldspar. The occurrence patterns of different fluid types within various pore-throat structures were established, revealing the relationships among mineral composition, pore size, pore-throat structure, and fluid distribution. These findings provide valuable insights into the pore structure and fluid distribution of tight sandstone reservoirs, enhancing the understanding of fluid behavior in unconventional systems.
流体类型和含量直接控制致密储层中的流体流动性。目前,流体类型有两种分类方式。一种是将流体分为可动流体(MF)、毛管束缚流体(CAF)和黏土束缚流体(CLF)。另一种是将流体分为自由流体和吸附流体。然而,这两种流体分类方案之间的内在关系仍不明确。为了研究孔隙结构和流体类型特征,对陇东地区长7致密砂岩进行了一系列实验。通过将低温氮吸附(LTNA)与核磁共振(NMR)相结合,可以获得全尺度孔径分布(PSD)。长7致密砂岩的PSD主要范围为1纳米至20微米。基于分形特征,孔隙系统分为大孔(主要>150.8纳米)和微孔(主要<150.8纳米)。MF、CLF和CAF分别占总流体的11.1 - 49.7%(平均34.6%)、17.3 - 40.1%(平均26.7%)和32.9 - 48.8%(平均38.7%)。此外,大孔与MF呈正相关,与CAF和CLF呈负相关,而微孔则呈现相反的趋势。通过将NMR数据与理论模型相结合,建立了两种流体分类方法之间的明确对应关系:MF和CAF与自由流体密切对应,而CLF与吸附流体密切相关。值得注意的是,在低孔隙度和极细孔喉的样品中,离心和理论模型的结合可能会低估实际的自由流体含量。MF与石英和黏土矿物呈弱负相关;CAF和CLF与石英和黏土呈弱正相关,但与长石呈负相关。建立了不同流体类型在各种孔喉结构中的赋存模式,揭示了矿物组成、孔径、孔喉结构和流体分布之间的关系。这些发现为致密砂岩储层的孔隙结构和流体分布提供了有价值的见解,加深了对非常规系统中流体行为的理解。