使用糖自动分析仪的分析柱进行制备，以分离相同分子量的低聚葡萄糖。

Preparative use of the analytical column of a sugar autoanalyzer for resolution of gluco-oligosaccharides of the same molecular weight.

作者信息

Torii M, Alberto B P, Tanaka S, Tsumuraya Y, Misaki A, Sawai T

出版信息

J Biochem. 1979 Mar;85(3):883-6.

Abstract

A sugar autoanalyzer was used on a preparative scale to resolve a gluco-oligosaccharide mixture. In this way the components of the following mixtures were resolved: O-alpha-D-glucopyranosyl-(1-3)-O-[alpha-D-glucopyranosyl-(1-6)]-D-glucose (1), O-alpha-D-glucopyranosyl-(1-6)-O-alpha-D-glucopyranosyl-(1-3)-D-glucose (2) and O-alpha-D-glucopyranosyl-(1-3)-O-alpha-D-glucopyranosyl-(1-6)-D-glucose (3), O-alpha-D-glucopyranosyl-(1-3)-O-alpha-D-glucopyranosyl-(1-4)-D-glucose (4) and O-alpha-D-glucopyranosyl-(1-4)-O-alpha-D-glucopyranosyl-(1-3)-D-glucose (5), and O-alpha-D-glucopyranosyl-(1-2)-O-alpha-D-glucopyranosyl-(1-6)-O-alpha-D-glucopranosyl-(1-6)-O-alpha-D-glucopyranosyl-(1-6)-D-glucose (6) and O-alpha-D-glucopyranosyl-(1-3)--O-alpha-D-glucopyranosyl-(1-6)-O-alpha-D-glucopyranosyl-(1-6)-O-alpha-D-glucopyranosyl-(1-6)-D-glucose (7).

摘要

使用一台制备规模的糖自动分析仪来分离低聚葡萄糖混合物。通过这种方式，分离出了以下混合物的成分：O-α-D-吡喃葡萄糖基-(1→3)-O-[α-D-吡喃葡萄糖基-(1→6)]-D-葡萄糖（1）、O-α-D-吡喃葡萄糖基-(1→6)-O-α-D-吡喃葡萄糖基-(1→3)-D-葡萄糖（2）和O-α-D-吡喃葡萄糖基-(1→3)-O-α-D-吡喃葡萄糖基-(1→6)-D-葡萄糖（3）、O-α-D-吡喃葡萄糖基-(1→3)-O-α-D-吡喃葡萄糖基-(1→4)-D-葡萄糖（4）和O-α-D-吡喃葡萄糖基-(1→4)-O-α-D-吡喃葡萄糖基-(1→3)-D-葡萄糖（5），以及O-α-D-吡喃葡萄糖基-(1→2)-O-α-D-吡喃葡萄糖基-(1→6)-O-α-D-吡喃葡萄糖基-(1→6)-O-α-D-吡喃葡萄糖基-(1→6)-D-葡萄糖（6）和O-α-D-吡喃葡萄糖基-(1→3)-O-α-D-吡喃葡萄糖基-(1→6)-O-α-D-吡喃葡萄糖基-(1→6)-O-α-D-吡喃葡萄糖基-(1→6)-D-葡萄糖（7）。