Von Dreele P H, Scheraga H A, Dyckes D F, Ferger M F, Du Vigneaud V
Proc Natl Acad Sci U S A. 1972 Nov;69(11):3322-6. doi: 10.1073/pnas.69.11.3322.
The peaks in the proton nuclear magnetic resonance spectrum of deamino-lysine-vasopressin in aqueous solution at pH values between 3 and 5 were assigned to particular amino-acid residues by use of the results of transfer-of-saturation studies, NH-C(alpha)H and C(alpha)H-C(beta)H decoupling experiments, and other data. The conformation of deamino-lysine-vasopressin in water differs from that of lysine-vasopressin in the same solvent.
通过饱和转移研究结果、NH-C(α)H和C(α)H-C(β)H去耦实验及其他数据,将pH值在3至5之间的水溶液中脱氨基赖氨酸加压素的质子核磁共振谱峰归属于特定的氨基酸残基。水中脱氨基赖氨酸加压素的构象与相同溶剂中赖氨酸加压素的构象不同。